3,6-二溴噻吩[3,2-b]噻吩合成路线 (共 7 条)
反应条件
lithium diisopropyl amide in tetrahydrofuran
参考文献
Biniek, Laure; Schroeder, Bob C.; Donaghey, Jenny E.; Yaacobi-Gross, Nir; Ashraf, Raja Shahid; Soon, Ying W.; Nielsen, Christian B.; Durrant, James R.; Anthopoulos, Thomas D.; McCulloch, Iain
Macromolecules, 2013 , vol. 46, # 3 p. 727 - 735
反应条件
acetic acid; zinc 1 h; Heating;
参考文献
Fuller, Lance S.; Iddon, Brian; Smith, Kevin A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3465 - 3470
反应条件
1: Br2 / CHCl3 2: Zn; AcOH View Scheme
参考文献
Biniek, Laure; Schroeder, Bob C.; Donaghey, Jenny E.; Yaacobi-Gross, Nir; Ashraf, Raja Shahid; Soon, Ying W.; Nielsen, Christian B.; Durrant, James R.; Anthopoulos, Thomas D.; McCulloch, Iain
Macromolecules, 2013 , vol. 46, # 3 p. 727 - 735
反应条件
1: 78 percent / LDA, Br2 / tetrahydrofuran; hexane / 1.) -80 deg C, 5 min, 2.) -80 deg C to r.t. 2: 76 percent / Zn, AcOH / 1 h / Heating View Scheme
参考文献
Fuller, Lance S.; Iddon, Brian; Smith, Kevin A.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 22 p. 3465 - 3470
反应条件
potassium iodide; copper(II) oxide in methanol
15 h; Inert atmosphereReflux;
参考文献
Hergue, Noemie; Frere, Pierre; Roncali, Jean
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 2 p. 588 - 595
反应条件
sodium methylate; potassium iodide; copper(II) oxide
参考文献
Turbiez, Mathieu; Frere, Pierre; Leriche, Philippe; Mercier, Nicolas; Roncali, Jean
Chemical Communications, 2005 , # 9 p. 1161 - 1163
参考文献
Ocean's King Lighting Science and Technology Co., Ltd.; Zhou, Mingjie; Huang, Jie; Liu, Hui
Patent: US8779204 B2, 2014 ;
Location in patent: Page/Page column ;