2,3-二氯-6-甲基喹喔啉合成路线 (共 6 条)
反应条件
thionyl chloride; N,N-dimethyl-formamide in 1,2-dichloro-ethane 2 h; Reflux;
参考文献
Romer, Duane R.
Journal of Heterocyclic Chemistry, 2009 , vol. 46, # 2 p. 317 - 319
反应条件
1: 87 percent / conc. HCl / H2O / 0.33 h / 100 °C 2: 87 percent / SOCl2, DMF / 1.5 h / Heating View Scheme
参考文献
Nakhi, Ali; Rahman, Md. Shafiqur; Kishore, Ravada; Meda, Chandana Lakshmi T.; Deora, Girdhar Singh; Parsa, Kishore V.L.; Pal, Manojit
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 20 p. 6433 - 6441
参考文献
Hinsberg
Chemische Berichte, 1883 , vol. 16, p. 1532
Justus Liebigs Annalen der Chemie, 1887 , vol. 237, p. 350
参考文献
Hinsberg
Chemische Berichte, 1883 , vol. 16, p. 1532
Justus Liebigs Annalen der Chemie, 1887 , vol. 237, p. 350
反应条件
potassium permanganate in water Heating;
参考文献
Obafemi, Craig A.; Pfleiderer, Wolfgang
Helvetica Chimica Acta, 1994 , vol. 77, # 6 p. 1549 - 1556
反应条件
sodium hydrogensulfide in ethanol
参考文献
Sonawane, Yogesh A.; Rajule, Rajkumar N.; Shankarling, Ganapati S.
Monatshefte fur Chemie, 2010 , vol. 141, # 10 p. 1145 - 1151