3-(3,4-二甲氧基苯基)-1-丙醇合成路线 （共 29 条）
反应条件
1: 81 percent / piperidine; pyridine / 6 h / 120 °C
2: 100 percent / H2 / Pd/C / ethanol / 1 h / 1551.44 Torr
3: 65.7 percent / NaBH4; TiCl4 / 1,2-dimethoxy-ethane / 18 h / 20 °C
View Scheme
参考文献
Sharma; Rathee, Raman
Journal of the Indian Chemical Society, 2005 , vol. 82, # 10 p. 938 - 939
反应条件
1: LiAlH4 / tetrahydrofuran / 1 h / -30 °C
2: H2 / 10percent Pd-charcoal / methanol / 2 h / 1810.02 Torr
View Scheme
参考文献
Enoki, Akio; Yajima, Yasuo; Gold, Michael H.
Phytochemistry (Elsevier), 1981 , vol. 20, # 6 p. 1543 - 1546
反应条件
1: aq. HCl / 6 h / Heating
2: H2 / 10percent Pd/C / methanol / 0.5 h / 760 Torr / Ambient temperature
3: LiBH4 / diethyl ether; toluene / 0.25 h / Heating
View Scheme
参考文献
Lam, Thi Bach Tuyet; Iiyama, Kenji; Stone, Bruce A.
Phytochemistry (Elsevier), 1992 , vol. 31, # 4 p. 1179 - 1184
反应条件
1: H2 / 10percent Pd/C / methanol / 0.5 h / 760 Torr / Ambient temperature
2: LiBH4 / diethyl ether; toluene / 0.25 h / Heating
View Scheme
参考文献
Lam, Thi Bach Tuyet; Iiyama, Kenji; Stone, Bruce A.
Phytochemistry (Elsevier), 1992 , vol. 31, # 4 p. 1179 - 1184
反应条件
lithium borohydride in diethyl ether; toluene
0.25 h; Heating;
参考文献
Lam, Thi Bach Tuyet; Iiyama, Kenji; Stone, Bruce A.
Phytochemistry (Elsevier), 1992 , vol. 31, # 4 p. 1179 - 1184
反应条件
1: 95 percent / H2 / Pd/C / dioxane / 3102.9 Torr
2: 65 percent / aq. HCl 6N / dioxane / 4 h / Heating
3: 90 percent / LiAlH4 / diethyl ether / 3 h / Heating
View Scheme
参考文献
Bellucci; Teodori; Gualtieri
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 10 p. 730 - 744
反应条件
hydrogen; palladium on activated charcoal
参考文献
Muehldorf, Alexander V.; Guzman-Perez, Angel; Kluge, Arthur F.
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8755 - 8758
反应条件
1: i-Pr2NH, (PPH3)2PdCl2, CuI
2: H2 / 10percent Pd/C
View Scheme
参考文献
Muehldorf, Alexander V.; Guzman-Perez, Angel; Kluge, Arthur F.
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8755 - 8758
反应条件
1: 65 percent / aq. HCl 6N / dioxane / 4 h / Heating
2: 90 percent / LiAlH4 / diethyl ether / 3 h / Heating
View Scheme
参考文献
Bellucci; Teodori; Gualtieri
Farmaco, Edizione Scientifica, 1985 , vol. 40, # 10 p. 730 - 744
反应条件
tri-n-butyl-tin hydride in benzene
3.5 h; Irradiation;
参考文献
Chowdhury, Nilanjana; Anoop, Anakuthil; Singh, N.D. Pradeep
Synthesis (Germany), 2012 , vol. 44, # 11 art. no. SS-2012-N1173-OP, p. 1745 - 1754
