4-氯-3,5-二硝基三氟甲苯合成路线 (共 44 条)
反应条件
hydrogen; Pd on carbon; palladium in methanol; water
参考文献
Occidental Chemical Corporation
Patent: US5347052 A1, 1994 ;
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Imperial Chemical Industries Limited
Patent: US4384135 A1, 1983 ;
反应条件
sodium hydroxide in hydrogenchloride; water
参考文献
The Upjohn Company
Patent: US3993679 A1, 1976 ;
反应条件
1: 69 percent / NaI, glacial acetic acid / acetone / 24 h / 63 - 65 °C 2: 77 percent / KF, o-phthaloyl dichloride / tetrahydrothiophene 1,1-dioxide / 24 h / 180 - 200 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 9 p. 1325 - 1331
参考文献
Nestler,H.J.; Bestian,H.
Justus Liebigs Annalen der Chemie, 1974 , p. 460 - 467
参考文献
Eli Lilly and Company
Patent: US3980784 A1, 1976 ;
反应条件
sodium formate; sodium acetate; palladium monocarbide in acetic acid
参考文献
Occidental Chemical Corporation
Patent: US5144076 A1, 1992 ;
反应条件
hydrogen; Pd on carbon; palladium in methanol; water
参考文献
Occidental Chemical Corporation
Patent: US5347052 A1, 1994 ;
反应条件
acetic acid; sodium iodide in acetone T=63 - 65°C; 24 h;
参考文献
Khalfina; Rogozhnikova; Vlasov
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 9 p. 1325 - 1331
反应条件
isobutyramide; copper T=100°C; 5 h;
参考文献
Clark, James H.; McClinton, Martin A.; Blade, Robert J.
Journal of the Chemical Society, Chemical Communications, 1988 , # 10 p. 638 - 639