2,6-二硝基-4-三氟甲酚合成路线 （共 12 条）
反应条件
sodium hydroxide in 1,4-dioxane; water 0.25 h; Heating;
参考文献
Bujan, Elba I.; Salum, Maria Laura
Canadian Journal of Chemistry, 2004 , vol. 82, # 8 p. 1322 - 1327
反应条件
sodium hydroxide in 1,4-dioxane; water 0.583333 h; Heating;
参考文献
Bujan, Elba I.; Salum, Maria Laura
Canadian Journal of Chemistry, 2004 , vol. 82, # 8 p. 1322 - 1327
反应条件
sodium hydroxide in dimethyl sulfoxide
参考文献
Chen, Mei-Jin; Chi, Ching-Sung; Chen, Qing-Yun
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 54, # 1/4 p. 87 - 93
反应条件
triethylamine in N,N-dimethyl-formamide 2.5 h; Ambient temperature;
参考文献
Chen, Mei-Jin; Chi, Ching-Sung; Chen, Qing-Yun
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 54, # 1/4 p. 87 - 93
反应条件
1: NaHCO3 / tetrahydrofuran / 0.5 h / Heating 2: Et3N / toluene / 6.5 h / Ambient temperature View Scheme
参考文献
Collins; McFarlane; Mackie; Smith
Tetrahedron, 1992 , vol. 48, # 37 p. 7887 - 7898
反应条件
triethylamine in toluene 6.5 h; Ambient temperature;
参考文献
Collins; McFarlane; Mackie; Smith
Tetrahedron, 1992 , vol. 48, # 37 p. 7887 - 7898
反应条件
sulfuric acid; water; nitric acid T=110°C;
参考文献
Jagupol'skii; Mospan
Ukrainskii Khimicheskii Zhurnal (Russian Edition), 1955 , vol. 21, p. 81,83
Chem.Abstr., 1955 , p. 8866
反应条件
oxygen; triethylamine in N,N-dimethyl-formamide 1.5 h; Ambient temperature;
参考文献
Chen, Mei-Jin; Chi, Ching-Sung; Chen, Qing-Yun
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 54, # 1/4 p. 87 - 93
反应条件
sodium hydroxide; water in 1,4-dioxane 18 h; Heating;
参考文献
Bujan, Elba I.; Salum, Maria Laura
Canadian Journal of Chemistry, 2004 , vol. 82, # 8 p. 1322 - 1327
反应条件
1: aqueous H2SO4; NaNO2 / anschliessendes Erhitzen mit CuSO4 2: HNO3; H2O; H2SO4 / 110 °C View Scheme
参考文献
Jagupol'skii; Mospan
Ukrainskii Khimicheskii Zhurnal (Russian Edition), 1955 , vol. 21, p. 81,83
Chem.Abstr., 1955 , p. 8866
