3,4-二羟基-5-甲氧基苯甲醛合成路线 （共 39 条）
反应条件
copper; sodium hydroxide in water 24 h; Heating;
参考文献
Pettit, George R.; Thornhill, Andrew; Melody, Noeleen; Knight, John C.
Journal of Natural Products, 2009 , vol. 72, # 3 p. 380 - 388
反应条件
sodium hydroxide; copper(II) sulfate in water Reflux;
参考文献
Altemoeller, Martina; Gehring, Timo; Cudaj, Judith; Podlech, Joachim; Goesmann, Helmut; Feldmann, Claus; Rothenberger, Alexander
European Journal of Organic Chemistry, 2009 , # 13 p. 2130 - 2140
反应条件
pyridine; aluminium trichloride in dichloromethane T=20°C; Demethylation; 72 h;
参考文献
Zouhiri, Fatima; Mouscadet, Jean-Francois; Mekouar, Khalid; Desmaele, Didier; Savoure, Delphine; Leh, Herve; Subra, Frederic; Le Bret, Marc; Auclair, Christian; D'Angelo, Jean
Journal of Medicinal Chemistry, 2000 , vol. 43, # 8 p. 1533 - 1540
反应条件
silver; sodium hydrogencarbonate; sodium iodide; zinc in ethylene glycol dimethyl ether; dimethyl sulfoxide T=60°C; 0.666667 h;
参考文献
Chung, Chi Kong; Ho, Mei Sing; Lun, Kue Sun; Wong, Man On; Wong, Henry N. C.; Tam, Shang Wai
Synthetic Communications, 1988 , vol. 18, # 5 p. 507 - 510
反应条件
1: glacial acetic acid / 25 °C / durch Bromierung 2: NaOH-solution; copper / 200 - 210 °C View Scheme
参考文献
Lam; Iiyama; Stone
Phytochemistry, 1996 , vol. 41, # 6 p. 1507 - 1510
反应条件
copper dichloride in N,N-dimethyl-formamide 2 h; Heating;
参考文献
Russell, Wendy R.; Burkitt, Mark J.; Scobbie, Lorraine; Chesson, Andrew
Bioorganic Chemistry, 2003 , vol. 31, # 3 p. 206 - 215
反应条件
1: 67 percent / bromine; acetic acid 2: 71 percent / copper(II) chloride / dimethylformamide / 2 h / Heating View Scheme
参考文献
Russell, Wendy R.; Burkitt, Mark J.; Scobbie, Lorraine; Chesson, Andrew
Bioorganic Chemistry, 2003 , vol. 31, # 3 p. 206 - 215
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Hoffmann-La Roche
Patent: DE350650 , 1930 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 566
反应条件
1: aq. NaOH solution 2: chloroform; phosphorus (V)-chloride 3: toluene; palladium/barium sulfate / 110 °C / Hydrogenation.Behandeln einer aethanol.Loesung des Reaktionsprodukts mit wss.NaOH unter Wasserstoff View Scheme
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1932 , vol. <2>133, p. 120,123,124
反应条件
aluminium(III) iodide; tetra-(n-butyl)ammonium iodide in cyclohexane 6 h; other reaction time, other molar ratios of educt/AlI3 and educt/catalyst; Product distribution;
参考文献
Andersson, Sven
Synthesis, 1985 , # 4 p. 437 - 439
