3,4-二羟基-5-甲氧基苯甲醛合成路线 (共 39 条)
反应条件
sodium carbonate in acetone 5 h; Heating;
参考文献
Synthetic Communications, , vol. 28, # 9 p. 1517 - 1524
参考文献
Kratzl; Billek
Holzforschung, 1953 , vol. 7, p. 66,69
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Kratzl et al.
Monatshefte fuer Chemie, 1954 , vol. 85, p. 1154,1160
反应条件
sorgum caffeic acid O-methyltransferase (Bmr-12); sulfolobus S-adenosylhomocysteine hydrolase in water; N,N-dimethyl-formamide T=37°C; pH=7.5; aq. bufferEnzymatic reaction; Kinetics;
参考文献
Palmer, Nathan A.; Sattler, Scott E.; Saathoff, Aaron J.; Sarath, Gautam
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 9 p. 5220 - 5226
反应条件
potassium carbonate in acetone 7 h; Reflux;
参考文献
Sun, Bing-Feng; Hong, Ran; Kang, Yan-Biao; Deng, Li
Journal of the American Chemical Society, 2009 , vol. 131, # 30 p. 10384 - 10385
反应条件
potassium carbonate in N,N-dimethyl-formamide 20 h; Heating; Yield given;
参考文献
Sharma, V. K.; Gupta, S. R.
Acta Chimica Hungarica, 1983 , vol. 114, # 3-4 p. 361 - 364
反应条件
1: With pyridine T=55°C; 2: With piperidine; aniline T=20°C;
参考文献
Russell, Wendy R.; Burkitt, Mark J.; Scobbie, Lorraine; Chesson, Andrew
Bioorganic Chemistry, 2003 , vol. 31, # 3 p. 206 - 215
反应条件
sodium carbonate in acetone 6 h; Reflux;
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
反应条件
sodium carbonate in acetone 5 h; Reflux;
参考文献
Cervi, Aymeric; Aillard, Paul; Hazeri, Nourallah; Petit, Laurent; Chai, Christina L. L.; Willis, Anthony C.; Banwell, Martin G.
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9876 - 9882
反应条件
sodium carbonate in acetone 5 h; Heating;
参考文献
Synthetic Communications, , vol. 28, # 9 p. 1517 - 1524
反应条件
1: K2CO3 / dimethylformamide / 4 h / 70 °C
2: NaBH4 / methanol / 0.17 h / 20 °C
3: PBr3 / diethyl ether / 1 h / 20 °C
View Scheme
参考文献
Sakakibara, Norikazu; Suzuki, Shiro; Umezawa, Toshiaki; Shimada, Mikio
Organic and biomolecular chemistry, 2003 , vol. 1, # 14 p. 2474 - 2485