2-己基-5-丙基苯-1,3-二醇合成路线 （共 7 条）
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile
48 h; Heating;
参考文献
Covarrubias-Zuniga, Adrian; Avila-Zarraga, Jose G.; Arias Salas, David
Synthetic Communications, 2003 , vol. 33, # 18 p. 3173 - 3181
反应条件
trimethylsilyl iodide in acetonitrile
24 h; Heating;
参考文献
Danheiser, Rick L.; Gee, Stephen K.
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1672 - 1674
反应条件
1: 55.6 percent / quinoline; CuO / 0.25 h / 215 °C
2: 89 percent / NaI; Me3SiCl / acetonitrile / 48 h / Heating
View Scheme
参考文献
Covarrubias-Zuniga, Adrian; Avila-Zarraga, Jose G.; Arias Salas, David
Synthetic Communications, 2003 , vol. 33, # 18 p. 3173 - 3181
反应条件
1: 90 percent / KOH / ethane-1,2-diol; H2O / 2 h / 115 - 120 °C
2: 55.6 percent / quinoline; CuO / 0.25 h / 215 °C
3: 89 percent / NaI; Me3SiCl / acetonitrile / 48 h / Heating
View Scheme
参考文献
Covarrubias-Zuniga, Adrian; Avila-Zarraga, Jose G.; Arias Salas, David
Synthetic Communications, 2003 , vol. 33, # 18 p. 3173 - 3181
反应条件
trimethylsilyl iodide; N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium
1) Et2O, 2) CH3CN, heating; Yield given. Multistep reaction;
参考文献
Kotnis, Atul S.
Tetrahedron Letters, 1991 , vol. 32, # 29 p. 3441 - 3444
反应条件
1: (i) Et2O, (ii) H2, Pd-C, AcOEt
View Scheme
参考文献
Achenbach; Kohl; Kunze
Chemische Berichte, 1979 , vol. 112, # 5 p. 1841 - 1848
参考文献
Achenbach; Kohl; Kunze
Chemische Berichte, 1979 , vol. 112, # 5 p. 1841 - 1848
