3-(3-羟基苯基)丙-2-烯酸甲酯合成路线 （共 8 条）
反应条件
ethanol; hydroxylamine
参考文献
Justus Liebigs Annalen der Chemie, , vol. 389, p. 36,111
反应条件
sulfuric acid
Fischer–Speier Esterification; 20 h; Reflux;
参考文献
Guzman, Juan D.; Mortazavi, Parisa N.; Munshi, Tulika; Evangelopoulos, Dimitrios; McHugh, Timothy D.; Gibbons, Simon; Malkinson, John; Bhakta, Sanjib
MedChemComm, 2014 , vol. 5, # 1 p. 47 - 50
反应条件
1,1'-bis(di-tert-butylphosphino)ferrocene palladium dichloride; N,N-dicyclohexylmethylamine; 4,4'-di-tert-butylbiphenyl; tetrabutyl-ammonium chloride in N,N-dimethyl acetamide
T=80°C; Heck Reaction; 24 h; Glovebox; Reagent/catalyst;
参考文献
Murray, Paul M.; Bower, John F; Cox, David K; Galbraith, Ewan K; Parker, Jeremy S; Sweeney, Joseph B.
Organic Process Research and Development, 2013 , vol. 17, # 3 p. 397 - 405
反应条件
in methanol
T=60°C; Esterification; 1 h;
参考文献
Daayf, Fouad; Ongena, Marc; Boulanger, Renald; El Hadrami, Ismail; Belanger, Richard R.
Journal of Chemical Ecology, 2000 , vol. 26, # 7 p. 1579 - 1593
参考文献
Kwon, Byoung-Mog; Lee, Seung-Ho; Cho, Young-Kwon; Bok, Song-Hae; So, Seung-Ho; Youn, Mi-Ran; Chang, Soo-Ik
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 19 p. 2473 - 2476
反应条件
1: SnCl2; hydrochloric acid / ueber mehrerer Stufen
2: sodium acetate / Verseifung der entstandenen Acetyl-m-cumarsaeure mit Alkalilauge
3: methanol; KOH
View Scheme
参考文献
Rieche
Chemische Berichte, 1889 , vol. 22, p. 2354
反应条件
1: sodium acetate / Verseifung der entstandenen Acetyl-m-cumarsaeure mit Alkalilauge
2: methanol; KOH
View Scheme
参考文献
Rieche
Chemische Berichte, 1889 , vol. 22, p. 2354
反应条件
methanol; potassium hydroxide
参考文献
Rieche
Chemische Berichte, 1889 , vol. 22, p. 2354
