2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖合成路线 (共 199 条)
反应条件
potassium carbonate in dichloromethane 48 h; Ambient temperaturevarious times; Product distribution;
参考文献
Schmidt, Richard R.; Michel, Josef; Roos, Michael
Liebigs Annalen der Chemie, 1984 , # 7 p. 1343 - 1357
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane
参考文献
Bellucci, Maria Cristina; Terraneo, Giancarlo; Volonterio, Alessandro
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 15 p. 2421 - 2444
反应条件
1: pyridine 2: MeONa / methanol; pyridine / 2.5 h / 80 °C View Scheme
参考文献
Wisniewski, Andrzej; Madaj, Janusz; Skorupowa, Eugenia; Sokolowski, Janusz
Journal of Carbohydrate Chemistry, 1994 , vol. 13, # 6 p. 873 - 880
反应条件
1.1: 83.9 percent / Cs2CO3 / CH2Cl2 / 30 h / 20 °C 2.1: molecular sieves 4 Angstroem / 1,2-dichloro-ethane / 1.5 h / 20 °C 2.2: 66.2 percent / trimethylsilyl triflate / 1,2-dichloro-ethane / 0.25 h / -18 °C 3.1: acetic acid; H2O / 45 °C 4.1: pyridine 5.1: 89.7 percent / Na / methanol / 1.5 h View Scheme
参考文献
Bukowski, Ralph; Morris, Laura M.; Woods, Robert J.; Weimar, Thomas
European Journal of Organic Chemistry, 2001 , # 14 p. 2697 - 2705
反应条件
1: mercuric cyanide 2: sodium methoxyde / methanol / 0.5 h / Heating View Scheme
参考文献
Parrish, Frederick W.; Meagher, Michael M.; Reilly, Peter J.
Carbohydrate Research, 1987 , vol. 168, p. 129 - 135
反应条件
1-bromo-N,N,2-trimethyl-1-propen-1-amine in chloroform 6 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 30, # 23 p. 3081 - 3084
反应条件
Ph3P*HClO4; triphenylphosphine in dichloromethane Ambient temperature;
参考文献
Maeda, Hatsuo; Matsumoto, Sayaka; Koide, Takashi; Ohmori, Hidenobu
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 6 p. 939 - 943
反应条件
trifluoroacetic anhydride in dichloromethane
参考文献
Leroux, Jacques; Perlin, Arthur S.
Carbohydrate Research, 1981 , vol. 94, p. 108 - 114
反应条件
tributylphosphine; 4 A molecular sieve; boron trifluoride diethyl etherate in acetonitrile 5 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Li; Sun; Landry; Zhao
Carbohydrate Research, 1995 , vol. 275, # 1 p. 179 - 184