2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖合成路线 （共 199 条）
反应条件
tin(IV) chloride in dichloromethane; N,N-dimethyl-formamide T=20°C; 24 h; Solvent;
参考文献
Sahoo, Laxminarayan; Singhamahapatra, Anadi; Paul, Katuri J.V.; Loganathan, Duraikkannu
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5361 - 5365
反应条件
tri-n-butyltin methoxide in toluene T=110°C; 1.5 h;
参考文献
Nudelman, Abraham; Herzig, Jacob; Gottlieb, Hugo E.; Keinan, Ehud; Sterling, Jeffrey
Carbohydrate Research, 1987 , vol. 162, p. 145 - 152
反应条件
trimethylsilylazide; tetra-n-butylammonium difluorotriphenylsilicate(IV) in tetrahydrofuran T=65°C; Substitution; hydrolysis; 20 h;
参考文献
Soli, Eric D.; DeShong, Philip
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9724 - 9726
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol T=30 - 35°C; 0.833333 h; Irradiation;
参考文献
Praly, Jean-Pierre; Ardakani, Azin Salek; Bruyere, Isabelle; Marie-Luce, Chrystelle; Bing Qin, Bing
Carbohydrate Research, 2002 , vol. 337, # 18 p. 1623 - 1632
反应条件
trifluoroacetic acid in dichloromethane Elimination; 0.5 h;
参考文献
Helliwell, Madeleine; Phillips, Iain M.; Pritchard, Robin G.; Stoodley, Richard J.
Tetrahedron Letters, 1999 , vol. 40, # 49 p. 8651 - 8655
反应条件
2,2'-azo-bisisobutyronitrile; tributyltin chloride; sodium cyanoborohydride in tert-butyl alcohol T=30 - 35°C; 0.75 h; Irradiation; Further byproducts given;
参考文献
Praly, Jean-Pierre; Ardakani, Azin Salek; Bruyere, Isabelle; Marie-Luce, Chrystelle; Bing Qin, Bing
Carbohydrate Research, 2002 , vol. 337, # 18 p. 1623 - 1632
反应条件
mercury(II) cyanide in nitromethane; benzene T=45°C; 5 h;
参考文献
Couto, Alicia; Lederkremer, Rosa M. De
Carbohydrate Research, 1984 , vol. 126, p. 313 - 320
反应条件
thionyl chloride; 2,2'-azo-bisisobutyronitrile in tetrachloromethane T=77°C; 2 h;
参考文献
Praly; Descotes
Tetrahedron Letters, 1990 , vol. 31, # 8 p. 1133 - 1136
反应条件
trichloromonobromomethane in tetrachloromethane Irradiation;
参考文献
Praly; Descotes
Tetrahedron Letters, 1990 , vol. 31, # 8 p. 1133 - 1136
反应条件
acetic acid; ethylenediamine in tetrahydrofuran Title compound not separated from byproducts;
参考文献
Zhang, Jian; Kovac, Pavol
Journal of Carbohydrate Chemistry, 1999 , vol. 18, # 4 p. 461 - 469
