2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖合成路线 （共 199 条）
反应条件
N-iodo-succinimide; trifluorormethanesulfonic acid in dichloromethane; water 16 h;
参考文献
Ramakrishnan, Archana; Pornsuriyasak, Papapida; Demchenko, Alexei V.
Journal of Carbohydrate Chemistry, 2005 , vol. 24, # 4-6 p. 649 - 663
反应条件
N-iodo-succinimide; trifluorormethanesulfonic acid in dichloromethane; water 16 h;
参考文献
Ramakrishnan, Archana; Pornsuriyasak, Papapida; Demchenko, Alexei V.
Journal of Carbohydrate Chemistry, 2005 , vol. 24, # 4-6 p. 649 - 663
反应条件
1: 85 percent / DMDO / acetone / 1 h / 20 °C 2: 84 percent / aq. HClO4 / 0.17 h / 0 °C 3: 52 percent / NaBH3CN; glacial acetic acid 4: 82 percent / (COCl)2; DMF / CH2Cl2 / 0.5 h 5: NaN3 / tetrahydrofuran / 4 h View Scheme
参考文献
Larsen, David S.; Lins, Roger J.; Stoodley, Richard J.; Trotter, Nicholas S.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2204 - 2212
反应条件
1: 84 percent / aq. HClO4 / 0.17 h / 0 °C 2: 52 percent / NaBH3CN; glacial acetic acid 3: 82 percent / (COCl)2; DMF / CH2Cl2 / 0.5 h 4: NaN3 / tetrahydrofuran / 4 h View Scheme
参考文献
Larsen, David S.; Lins, Roger J.; Stoodley, Richard J.; Trotter, Nicholas S.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2204 - 2212
反应条件
1: 52 percent / NaBH3CN; glacial acetic acid 2: 82 percent / (COCl)2; DMF / CH2Cl2 / 0.5 h 3: NaN3 / tetrahydrofuran / 4 h View Scheme
参考文献
Larsen, David S.; Lins, Roger J.; Stoodley, Richard J.; Trotter, Nicholas S.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2204 - 2212
反应条件
1: 82 percent / (COCl)2; DMF / CH2Cl2 / 0.5 h 2: NaN3 / tetrahydrofuran / 4 h View Scheme
参考文献
Larsen, David S.; Lins, Roger J.; Stoodley, Richard J.; Trotter, Nicholas S.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 18 p. 2204 - 2212
反应条件
1: sodium acetate / acetic anhydride / 2 h / 100 °C 2: hydrazinium monoacetate / N,N-dimethyl-formamide / 0.33 h / 50 °C View Scheme
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (CNRS); PIERRE FABRE MEDICAMENT
Patent: US2012/77777 A1, 2012 ;
反应条件
acetone; silver carbonate
参考文献
Schlubach; Gilbert
Chemische Berichte, 1930 , vol. 63, p. 2292,2297
反应条件
perchloric acid 0.25 h; Ambient temperature;
参考文献
Van Ameijde, Jeroen; Albada, H. Bauke; Liskamp, Rob M.J.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 8 p. 1042 - 1049
参考文献
Aspinall, Ian H.; Cowley, Phillip M.; Mitchell, Glynn; Stoodley, Richard J.
Journal of the Chemical Society, Chemical Communications, 1993 , # 15 p. 1179 - 1180
