2-氨基-3-环丁基丙酸乙酯合成路线 （共 12 条）
反应条件
1: CH2Cl2 / 12 h / 20 °C
2: LiOH*H2O / tetrahydrofuran; H2O / 3 h / 20 °C
3: 15.0 g / BOP; N-methylmorpholine / CH2Cl2 / 16 h / 20 °C
4: 14 g / LiAlH4 / tetrahydrofuran / 1 h / 20 °C
5: Et3N / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
MSN LABORATORIES LIMITED; THIRUMALAI RAJAN, Srinivasan; ESWARAIAH, Sajja; VENKAT REDDY, Ghojala; SAHADEVA REDDY, Maramreddy
Patent: WO2014/61034 A1, 2014 ;
反应条件
1: CH2Cl2 / 12 h / 20 °C
2: LiOH*H2O / tetrahydrofuran; H2O / 3 h / 20 °C
3: 15.0 g / BOP; N-methylmorpholine / CH2Cl2 / 16 h / 20 °C
View Scheme
参考文献
MSN LABORATORIES LIMITED; THIRUMALAI RAJAN, Srinivasan; ESWARAIAH, Sajja; VENKAT REDDY, Ghojala; SAHADEVA REDDY, Maramreddy
Patent: WO2014/61034 A1, 2014 ;
