6-甲基-4-苯并二氢呋喃-4-酮合成路线 （共 23 条）
反应条件
1: 68 percent / sodium borohydride; nickel(II) chloride hexahydrate / methanol; H2O / 4 h / 20 °C View Scheme
参考文献
Khurana, Jitender Mohan; Sharma, Purnima
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 3 p. 549 - 552
参考文献
Dann et al.
Justus Liebigs Annalen der Chemie, 1954 , vol. 587, p. 16,36
反应条件
1: conc. HCl / 8 h / Heating 2: 60 percent / PPA View Scheme
参考文献
Khanna, J. M.; Tandon, V. K.; Kar, K.; Sur, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 71 - 77
反应条件
2: concentrated sulfuric acid / 20 °C View Scheme
参考文献
Krollpfeiffer; Schultze
Chemische Berichte, 1924 , vol. 57, p. 207
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane 8 h; Heating;
参考文献
Shanker, Ch. Gouri; Mallaiah, B. Veera; Srimannarayana, G.
Synthesis, 1983 , # 4 p. 310 - 311
反应条件
1: pyridine / 24 h / 20 °C 2: palladium 10 on activated carbon; ammonia; hydrogen / methanol / 1 h / 20 °C / 3102.97 Torr View Scheme
参考文献
Schmidt, Robert G.; Bayburt, Erol K.; Latshaw, Steven P.; Koenig, John R.; Daanen, Jerome F.; McDonald, Heath A.; Bianchi, Bruce R.; Zhong, Chengmin; Joshi, Shailen; Honore, Prisca; Marsh, Kennan C.; Lee, Chih-Hung; Faltynek, Connie R.; Gomtsyan, Arthur
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 5 p. 1338 - 1341
反应条件
aluminium trichloride (heating);
参考文献
Misra,C.; Ghosh,A.
Synthetic Communications, 1978 , vol. 8, # 6 p. 403 - 408
反应条件
1: bromine / CHCl3 / Ambient temperature 2: 90 percent / triethylamine / methanol / 0.75 h / Ambient temperature View Scheme
参考文献
Sriram; Srinivasan; Santhosh; Balasubramanian
Acta Crystallographica Section C: Crystal Structure Communications, 1997 , vol. 53, # 8 p. 1073 - 1075
反应条件
palladium (II) trifluoroacetate; Cu(TFA)2*xH2O; silver(I) acetate
T=100°C; Heck Reaction; 48 h; Inert atmosphere; regioselective reaction;
参考文献
Moon, Youngtaek; Kwon, Daeil; Hong, Sungwoo
Angewandte Chemie, International Edition, 2012 , vol. 51, # 45 p. 11333 - 11336,4
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium hydrogencarbonate; [(t-Bu)3PH]BF4 in water
T=100°C; 3 h; Inert atmosphere; chemoselective reaction;
参考文献
Lessi, Marco; Masini, Tiziana; Nucara, Luca; Bellina, Fabio; Rossi, Renzo
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 501 - 507
