(S)-2-lt;N-(3'-tert-butylsalicylidene)aminogt;-3-methyl-1-butanol titanium tetraisopropoxide in dichloromethane T=-80°C; 36 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Aspinall, Helen C.; Greeves, Nicholas; Smith, Peter M.
Tetrahedron Letters, 1999 , vol. 40, # 9 p. 1763 - 1766
1: With Y(1,3-bis(2-methylferrocenyl)propane-1,3-dione)3 in dichloromethane T=-78°C; silylcyanation; 0.5 h; 2: With hydrogenchloride in tetrahydrofuran Hydrolysis;