2-叔丁基硫基-1,3-苯并噻唑合成路线 （共 6 条）
反应条件
CuO; potassium carbonate in N,N-dimethyl-formamide
T=140°C; 48 h; Inert atmosphereSchlenk technique;
参考文献
Rosario, Alisson R.; Casola, Kamila K.; Oliveira, Carla E.S.; Zeni, Gilson
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 14-15 p. 2960 - 2966
反应条件
1: carbon disulfide; 2-methylpropane-2-thiol With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 1 h;
2: 2-iodo aniline With copper(I) bromide in N,N-dimethyl-formamide
T=110°C; 6 h;
参考文献
Shi, Liu; Liu, Xiangqian; Zhang, Hui; Jiang, Yongwen; Ma, Dawei
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 4200 - 4204
反应条件
2,6-dimethoxy-p-benzoquinone in chloroform
T=20°C; 18 h;
参考文献
Mukaiyama, Teruaki; Ikegai, Kazuhiro
Chemistry Letters, 2004 , vol. 33, # 11 p. 1522 - 1523
反应条件
in tetrahydrofuran
T=0°C; 1 h;
参考文献
Nagasaki, Izuru; Matsumoto, Miyuki; Yamashita, Masanori; Miyashita, Akira
Heterocycles, 1999 , vol. 51, # 5 p. 1015 - 1024
反应条件
in 1,4-dioxane
T=20°C; 0.333333 h;
参考文献
Yu, Yanfei; Li, Zhengning; Jiang, Lan
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 5 p. 632 - 640
反应条件
sodium hydride
1.) THF, room temperature, 1 h, 2.) THF, reflux, 2.5 h; Yield given. Multistep reaction;
参考文献
Becher, Jan; Lundsgaard, John
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 14, p. 131 - 138
