2-苯基-2-环戊烯-1-酮合成路线 （共 43 条）
反应条件
tri-ruthenium(0)dodecacarbonyl in toluene
T=100°C; Pauson-Khand reaction; P=760 Torr;
参考文献
Itami, Kenichiro; Mitsudo, Koichi; Fujita, Kazuyoshi; Ohashi, Youichi; Yoshida, Jun-Ichi
Journal of the American Chemical Society, 2004 , vol. 126, # 35 p. 11058 - 11066
反应条件
sodium carbonate; palladium on activated charcoal in ethylene glycol dimethyl ether; water
T=25°C; Suzuki-Miyaura cross-coupling; 12 h;
参考文献
Felpin, Francois-Xavier
Journal of Organic Chemistry, 2005 , vol. 70, # 21 p. 8575 - 8578
反应条件
tributylphosphine; N-ethyl-N,N-diisopropylamine in dichloromethane; tert-butyl alcohol
T=25°C;
参考文献
Koech, Phillip K.; Krische, Michael J.
Journal of the American Chemical Society, 2004 , vol. 126, # 17 p. 5350 - 5351
反应条件
[Co4(CO)11{P(OPh)3}]
T=85°C; Cycloaddition; Pauson-Khand reaction; P=152000 - 159600 Torr; 46 h;
参考文献
Jeong, Nakcheol; Hwang, Sung Hee
Angewandte Chemie - International Edition, 2000 , vol. 39, # 3 p. 636 - 638
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=-45°C; 2 h;
参考文献
Wender, Paul A.; Erhardt, Jeanette M.; Letendre, Leo J.
Journal of the American Chemical Society, 1981 , vol. 103, # 8 p. 2114 - 2116
反应条件
4-methylmorpholine N-oxide in dichloromethane
T=20°C; Cycloaddition; Khand cycloadditions;
参考文献
Kerr, William J.; McLaughlin, Mark; Pauson, Peter L.; Robertson, Sarah M.
Journal of Organometallic Chemistry, 2001 , vol. 630, # 1 p. 104 - 117
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in water; toluene
Suzuki coupling; Reflux;
参考文献
Chiba, Shunsuke; Xu, Yan-Jun; Wang, Yi-Feng
Journal of the American Chemical Society, 2009 , vol. 131, # 36 p. 12886 - 12887
反应条件
1: With (x)BF4*C9H14NO(1+) in dichloromethane
T=-78°C; 1 h;
2: With sodium hydrogencarbonate in dichloromethane; water
T=20°C;
参考文献
Hayashi, Masaki; Shibuya, Masatoshi; Iwabuchi, Yoshiharu
Organic Letters, 2012 , vol. 14, # 1 p. 154 - 157
反应条件
tris(n-butyl)phosphine oxide in toluene
T=110°C; P=38000 Torr; 36 h;
参考文献
Billington, David C.; Helps, I. Malcolm; Pauson, Peter L.; Thomson, William; Willison, Debra
Journal of Organometallic Chemistry, 1988 , vol. 354, p. 233 - 242
反应条件
trimethylamine-N-oxide in methanol; toluene
T=45°C; Cycloaddition; Khand cycloaddition;
参考文献
Kerr, William J.; McLaughlin, Mark; Pauson, Peter L.; Robertson, Sarah M.
Journal of Organometallic Chemistry, 2001 , vol. 630, # 1 p. 104 - 117
