1-氯-4-(异氰基甲基)苯合成路线 （共 8 条）
反应条件
pyridine; polystyrene sulfonyl chloride resin in dichloromethane T=100°C; 0.166667 h; microwave irradiation;
参考文献
Launay, Delphine; Booth, Susan; Clemens, Ian; Merritt, Andrew; Bradley, Mark
Tetrahedron Letters, 2002 , vol. 43, # 40 p. 7201 - 7203
反应条件
1: With silver perchlorate in dichloromethane T=20°C; 1 h; 2: With sodium hydrogencarbonate in dichloromethane 0.166667 h;
参考文献
Kitano, Yoshikazu; Manoda, Tetsuya; Miura, Teppei; Chiba, Kazuhiro; Tada, Masahiro
Synthesis, 2006 , # 3 p. 405 - 410
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane; water 6 h;
参考文献
El Kaim, Laurent; Pinot-Perigord, Emmanuel
Tetrahedron, 1998 , vol. 54, # 15 p. 3799 - 3806
反应条件
1: 83 percent / 4 h / 0 - 20 °C 2: 1.) POCl3, Et3N, 2.) aq. Na2CO3 / 1.) CH2Cl2, 0 deg C, 1 h, 2.) CH2Cl2, 1 h View Scheme
参考文献
Jacobsen, E. Jon; Stelzer, Lindsay S.; Belonga, Kenneth L.; Carter, Donald B.; Im, Wha Bin; Sethy, Vimala H.; Tang, Andrew H.; Von Voigtlander, Philip F.; Petke, James D.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 19 p. 3820 - 3836
反应条件
2,6-dimethylpyridine in toluene T=80°C; Inert atmosphere;
参考文献
Dos Santos, Aurelie; El Kaim, Laurent; Grimaud, Laurence; Ronsseray, Caroline
Chemical Communications, 2009 , # 26 p. 3907 - 3909
反应条件
1: NaH / dimethylformamide 2: (i) aq. HCl, MeOH, (ii) NaOH View Scheme
参考文献
Matsumoto,K. et al.
Journal of Organic Chemistry, 1973 , vol. 38, p. 2094 - 2096
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=80°C; 1 h; relative rates, Hammett correlations and secondary α-deuterium kinetic isotope effect for cyanide abstractions from title comp. by tri-n-butyltin radical;
参考文献
Kim, Sung Soo; Yang, Ki Woong; Lee, Chang Soo
Journal of Organic Chemistry, 1996 , vol. 61, # 14 p. 4827 - 4829
反应条件
1,1-diphenylene; chlorobenzene in benzene T=170°C; also at 190, 210 and 230 deg C; ΔHY (excit.), ΔΔHY-H(excit.), ΔSY(excit.), ΔΔSY-H(excit); Rate constantThermodynamic data;
参考文献
Kim, Sung Soo; Choi, Won Jung; Zhu, Yu; Kim, Jin Hyun
Journal of Organic Chemistry, 1998 , vol. 63, # 4 p. 1185 - 1189
