5-(4-硝基苯磺酰)噻唑-2-胺合成路线 （共 8 条）
参考文献
Bambas
Journal of the American Chemical Society, 1945 , vol. 67, p. 668
反应条件
bromine; acetic acid anschliessend Erhitzen mit wss. Thioharnstoff;
参考文献
Ohta
Yakugaku Zasshi, 1948 , vol. 68, p. 216
Chem.Abstr., 1954 , p. 3966
Full Text Show Details
Izumi et al.
Yakugaku Zasshi, 1951 , vol. 71, p. 546,548
Chem.Abstr., 1952 , p. 497
反应条件
chloroform; chlorine anschliessend Erhitzen mit wss. Thioharnstoff;
参考文献
Izumi et al.
Yakugaku Zasshi, 1951 , vol. 71, p. 546,548
Chem.Abstr., 1952 , p. 497
反应条件
1: KMnO4; aqueous acetic acid 2: acetic acid; bromine / anschliessend Erhitzen mit wss. Thioharnstoff View Scheme
参考文献
Ohta
Yakugaku Zasshi, 1948 , vol. 68, p. 216
Chem.Abstr., 1954 , p. 3966
反应条件
1: sodium ethylate; ethanol 2: KMnO4; aqueous acetic acid 3: acetic acid; bromine / anschliessend Erhitzen mit wss. Thioharnstoff View Scheme
参考文献
Ohta
Yakugaku Zasshi, 1948 , vol. 68, p. 216
Chem.Abstr., 1954 , p. 3966
参考文献
Ohta
Yakugaku Zasshi, 1948 , vol. 68, p. 216
Chem.Abstr., 1954 , p. 3966
Show Details
Izumi et al.
Yakugaku Zasshi, 1951 , vol. 71, p. 546,548
Chem.Abstr., 1952 , p. 497
反应条件
potassium fluoride; polymethylhydrosiloxane; palladium diacetate in tetrahydrofuran; water
T=20°C; 0.5 h;
参考文献
Rahaim Jr., Ronald J.; Maleczka Jr., Robert E.
Synthesis, 2006 , # 19 p. 3316 - 3340
反应条件
ammonium chloride in tetrahydrofuran; ethanol; water
参考文献
Fujisawa Pharmaceutical Co., Ltd.
Patent: US5256675 A1, 1993 ;
