METHYLPHENYLSILANEDIOL合成路线 （共 11 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in tetrahydrofuran T=60°C; Arylation; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 17 p. 5342 - 5349
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in tetrahydrofuran T=60°C; Arylation; 12 h;
参考文献
Hirabayashi, Kazunori; Mori, Atsunori; Kawashima, Jun; Suguro, Masahiro; Nishihara, Yasushi; Hiyama, Tamejiro
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5342 - 5349
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in tetrahydrofuran T=60°C; Arylation; 5 h;
参考文献
Hirabayashi, Kazunori; Mori, Atsunori; Kawashima, Jun; Suguro, Masahiro; Nishihara, Yasushi; Hiyama, Tamejiro
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5342 - 5349
反应条件
phosphate buffer; palladium on activated charcoal in 1,4-dioxane
T=20°C; Oxidation; pH=6.84; 3 h;
参考文献
Hirabayashi, Kazunori; Mori, Atsunori; Kawashima, Jun; Suguro, Masahiro; Nishihara, Yasushi; Hiyama, Tamejiro
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5342 - 5349
反应条件
trifluoroacetic acid in dichloromethane
T=0°C; 2 h;
参考文献
Anderson, Thomas F.; Statham, Matthew A.J.; Carroll, Michael A.
Tetrahedron Letters, 2006 , vol. 47, # 20 p. 3353 - 3355
参考文献
Lasocki,Z.
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, 1964 , vol. 12, p. 281 - 287
参考文献
Schostakowskii et al.
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 3344,3351; engl.Ausg.S.3721,3724
反应条件
sodium tetrafluoroborate in various solvent(s)
T=200°C; 15 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Farooq, Omar
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 4 p. 661 - 665
反应条件
anhydrous magnesium carbonate
参考文献
Fukukawa
Kogyo Kagaku Zasshi, 1956 , vol. 59, p. 1206
Chem.Abstr., 1958 , p. 14558
参考文献
Sowa
Patent: US2486992 , 1945 ;
