反应条件
1.1: imid. 2.1: 78 percent / i-Pr2EtN 3.1: Bu3SnH; AIBN 3.2: SnBr4 / -78 °C 4.1: 80 percent / pyridine 5.1: 59 percent / Bu3SnH; AIBN 6.1: 91 percent / DDQ 7.1: 97 percent / Bu4NF 8.1: Dess-Martin periodinane 9.1: 99 percent / Dess-Martin periodinane 10.1: 74 percent / n-BuLi 11.1: DIBAL-H 12.1: Dess-Martin periodinane 13.1: 67 percent / Li(i-Pr)2N / -78 °C 14.1: 79 percent / Cl2CHCO2H 15.1: Dess-Martin periodinane 16.1: NaClO2 17.1: MgBr2; n-BuSH; K2CO3 18.1: 62 percent / 2,4,6-trichlorobenzoyl chloride; DMAP 19.1: 91 percent / CF3CO2H / CH2Cl2 20.1: DMDO / -50 °C View Scheme
参考文献
Martin, Nathaniel; Thomas, Eric J.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 39 p. 7952 - 7964
