2-溴-4-二甲基氨基吡啶合成路线 （共 4 条）
反应条件
1: With n-butyllithium; 2-(dimethylamino)-ethanol in hexane T=0°C; 1 h; 2: With carbon tetrabromide in hexane T=-78 - 0°C; 1.5 h; Further stages.;
参考文献
Cuperly, David; Gros, Philippe; Fort, Yves
Journal of Organic Chemistry, 2002 , vol. 67, # 1 p. 238 - 241
反应条件
in ethanol T=50°C; 5 h;
参考文献
PFIZER LIMITED
Patent: WO2007/57775 A1, 2007 ;
Location in patent: Page/Page column 159-160 ;
WO 2007/057775 A1
反应条件
4-(N,N-dimethlyamino)pyridine; n-butyllithium in hexane; water
参考文献
SOLVAY SA
Patent: US2012/25177 A1, 2012 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine in xylene
Stille cross-coupling reaction; 12 h; Heating;
参考文献
Cuperly, David; Gros, Philippe; Fort, Yves
Journal of Organic Chemistry, 2002 , vol. 67, # 1 p. 238 - 241
