Cp2Ti[P(OEt)3]2 in tetrahydrofuran 2.5 h; Product distribution;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3629917', constants.ctx, '0')">sodium hexamethyldisilazane</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '102391', constants.ctx, '0')">tetrahydrofuran</a> <br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 87 percent / BF₃*OEt₂ / toluene / 16 h / 20 &deg;C<br />2: 85 percent / NaBH₄ / 5 percent Pd/C / tetrahydrofuran; H₂O / 18 h / 20 &deg;C<br />3: 78 percent / NaHMDS / tetrahydrofuran / 16 h / 20 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: 87 percent / BF₃*OEt₂ / toluene / 16 h / 20 &deg;C<br />2: 85 percent / NaBH₄ / 5percent Pd/C / tetrahydrofuran; H₂O / 18 h / 20 &deg;C<br />3: 78 percent / NaHMDS / tetrahydrofuran / 16 h / 20 &deg;C<br /> <br /> &nbsp;