2,3-二甲基-2,3-二硝基丁烷合成路线 (共 158 条)
反应条件
lithium diisopropyl amide 1.) THF, hexane, -30 deg C, 5 min, 2.) HMPA, irradiation, 0-30 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russel, Glen A.; Mudryk, Boguslaw; Jawdosiuk, Mikolaj; Wrobel, Zbigniew
Journal of Organic Chemistry, 1982 , vol. 47, # 10 p. 1879 - 1884
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide 23 h; Irradiation;
参考文献
Bowman, W. Russell; Rakshit, Devajvoti; Valmas, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2327 - 2336
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide 22 h; Irradiation;
参考文献
Bowman, W. Russell; Rakshit, Devajvoti; Valmas, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2327 - 2336
反应条件
in dimethyl sulfoxide 2 h; Irradiation;
参考文献
Al-Khalil, Suleiman I.; Bowman, W. Russell
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2517 - 2520
反应条件
in N,N-dimethyl-formamide 2 h; Irradiation;
参考文献
Bowman, W. Russell; Richardson, Geoffrey D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1407 - 1413
反应条件
in N,N-dimethyl-formamide 5 h; Irradiation;
参考文献
Bowman, W. Russell; Richardson, Geoffrey D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1407 - 1413
反应条件
in dimethyl sulfoxide 4 h; Irradiation;
参考文献
Bowman, W. Russell; Richardson, Geoffrey D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1407 - 1413
参考文献
Shimomura, Osamu; Abe, Kazuhisa; Hirota, Minoru
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 795 - 798
反应条件
in dimethyl sulfoxide 0.25 h; Photolysis;
参考文献
Al-Khalil; Bowman; Gaitonde; Marley; Richardson
Journal of the Chemical Society, Perkin Transactions 2, 2001 , # 9 p. 1557 - 1565
反应条件
potassium tert-butylate in dimethyl sulfoxide 1.33333 h; Irradiationeffects of base ( tert-BuOK, tert-BuOLi, DNB), 18-Crown-6 and reraction time; Product distribution;
参考文献
Russell, Glen A.; Ros, Fransisco
Journal of the American Chemical Society, 1985 , vol. 107, # 8 p. 2506 - 2511