2,3-二甲基-2,3-二硝基丁烷合成路线 （共 158 条）
反应条件
ammonia; dihydrogen peroxide in water T=69.84 - 74.84°C; P=750.075 - 1875.19 Torr; Mechanism; Solvent;
参考文献
Wang, Yi; Zhang, Shengjian; Zhao, Yingxian; Lin, Min
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 385, p. 1 - 6
反应条件
potassium tert-butylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Ros, Francisco; Rosa, Jose de la
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2868 - 2870
反应条件
sodium dithionite; potassium carbonate; N,N'-dioctyl-4,4'-bipyridinium in dichloromethane; water T=35°C; 3 h;
参考文献
Park, Kwanghee Koh; Lee, Chul Woo; Choi, Sook Young
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 5 p. 601 - 604
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane; dimethyl sulfoxide T=35°C; 1.5 h; Irradiation;
参考文献
Russell, Glen A.; Mudryk, Boguslaw; Ros, Francisco; Jawdosiuk, Mikolaj
Tetrahedron, 1982 , vol. 38, # 8 p. 1059 - 1068
反应条件
sodium hydroxide; (NH4)2S2O8; sodium nitrite in water T=0 - 10°C;
参考文献
Russell
Journal of the American Chemical Society, 1954 , vol. 76, p. 1595
反应条件
sodium hydroxide; sodium peroxodisulphate; potassium hexacyanoferrate(III) in dichloromethane T=0°C; 1.25 h;
参考文献
Adebayo, Adelaide T. O. M.; Bowman, W. Russell; Salt, W. G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1415 - 1421
反应条件
Ethylphosphonat-mono-Na-salz in tetrahydrofuran Irradiation1.) -78 deg C, 1 h, 2.) 25 deg C, 1 h;
参考文献
Russel, Glen A.; Ros, Francisco; Hershberger, J.; Tashtoush, Hasan
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1480 - 1483
反应条件
in dimethyl sulfoxide T=20°C; 3 h;
参考文献
Zorin, V. V.; Kukovitskii, D. M.; Zlot-skii, S. S.; Todres, Z. V.; Rakhmankulov, D. L.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 4 p. 828 - 833,735 - 739
反应条件
in dimethyl sulfoxide T=20°C; 2 h; UV-irradiationInert atmosphere;
参考文献
Maillard-Boyer, Martine; Castera-Ducros, Caroline; Verhaeghe, Pierre; Sifredi, France; Rathelot, Pascal; Vanelle, Patrice
Molecules, 2010 , vol. 15, # 4 p. 2719 - 2729
反应条件
sodium hydroxide; sodium peroxodisulphate; potassium hexacyanoferrate(III) in dichloromethane T=0°C; 2 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Adebayo, Adelaide T. O. M.; Bowman, W. Russell; Salt, W. G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1415 - 1421
