2,3-二甲基-2,3-二硝基丁烷合成路线 (共 158 条)
反应条件
in 1,2,2-trifluoro-trichloroethane T=31°C;
参考文献
Zhao, Cheng-Xue; Chen, Guo-Fei; Jiang, Xi-Kui; Wang, Xian-Shan
Journal of Fluorine Chemistry, 1987 , vol. 35, p. 597 - 606
反应条件
sodium hydroxide; sodium peroxodisulphate; potassium hexacyanoferrate(III) in dichloromethane T=0°C; 1.25 h;
参考文献
Adebayo, Adelaide T. O. M.; Bowman, W. Russell; Salt, W. G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1415 - 1421
反应条件
sodium hydroxide; sodium peroxodisulphate; potassium hexacyanoferrate(III) in dichloromethane T=0°C; 1.25 h;
参考文献
Adebayo, Adelaide T. O. M.; Bowman, W. Russell; Salt, W. G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1415 - 1421
反应条件
in ethanol Irradiation;
参考文献
Russell,G.A. et al.
Journal of the American Chemical Society, 1971 , vol. 93, p. 5839 - 5845
反应条件
oxygen; 2-nitro-2-thiocyanatopropane in dimethyl sulfoxide 2 h;
参考文献
Al-Khalil, Suleiman I.; Bowman, W. Russell
Tetrahedron Letters, 1983 , vol. 24, # 24 p. 2517 - 2520
反应条件
sodium hydroxide; sodium peroxodisulphate; potassium hexacyanoferrate(III) in dichloromethane T=0°C; 1.25 h; Title compound not separated from byproducts;
参考文献
Adebayo, Adelaide T. O. M.; Bowman, W. Russell; Salt, W. G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1415 - 1421
反应条件
KNH2 in N,N,N',N',N'',N''-hexamethylphosphoric triamide 5 h;
参考文献
Ros, Francisco; Rosa, Jose de la
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2868 - 2870
反应条件
K(cryp 2.2.2)(1+) in dimethyl sulfoxide T=25°C; ion pairing and solvent effects;
参考文献
Russell, Glen A.; Ros, Francisco; Mudryk, Boguslaw
Journal of the American Chemical Society, 1980 , vol. 102, # 25 p. 7601 - 7603
反应条件
sodium hydroxide; potassium hexacyanoferrate(III) in diethyl ether T=0 - 10°C; 1 h;
参考文献
Bowman, W. Russell; Rakshit, Devajvoti; Valmas, Michael D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2327 - 2336
反应条件
isopropenylbenzene in methanol T=30°C; 48 h; Further byproducts given;
参考文献
Singh, P. R.; Khanna, R. K.
Tetrahedron Letters, 1982 , vol. 23, # 50 p. 5355 - 5358