4-乙酰氧基-3,5-二甲氧基苯甲酰氯合成路线 （共 16 条）
反应条件
thionyl chloride
Inert atmosphere;
参考文献
Yeun, Go Heum; Lee, Seung Hwan; Lim, Yong Bae; Lee, Hye Sook; Won, Moo-Ho; Lee, Bong Ho; Park, Jeong Ho
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 4 p. 1025 - 1029
反应条件
1: Et3N / dimethylformamide
2: SOCl2 / CHCl3 / Heating
View Scheme
参考文献
Gita, Haruhisa; Sobe, Yoshiaki; Akaku, Haruo; Ekine, Rena; Oto, Yuso; Isawa, Satoru; Hayashi, Hideya
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 4 p. 549 - 551
反应条件
1: sulfuric acid / 40 - 50 °C
2: pyridine
3: benzene; phosphorus pentachloride
View Scheme
参考文献
Bradley; Robinson
Journal of the Chemical Society, 1928 , p. 1551
反应条件
1: xylene; palladium/barium sulfate / 150 - 160 °C / Hydrogenation
View Scheme
参考文献
Imaki et al.
Nippon Nogei Kagaku Kaishi, 1944 , vol. 20, p. 289,292
Chem.Abstr., 1949 , p. 1743
反应条件
(i) NaH, (ii) /BRN= 3370542/; Multistep reaction;
参考文献
Pifferi; Monguzzi; Banfi; Carpi
Farmaco, Edizione Scientifica, 1973 , vol. 28, # 10 p. 818 - 829
反应条件
benzene
Behandeln des Reaktionsprodukts mit wss. KOH;
参考文献
Novelli
Ciencia, 1958 , vol. 18, p. 49
