反应条件
1: 69 percent / diethyl ether / 4 h / 36 - 38 °C 2: 60 percent / HCl / 2 h / Heating 3: 70 percent / p-TsOH / benzene / 15 h / Heating 4: 92 percent / LiAlH4 / diethyl ether / 5 h / Ambient temperature 5: 81 percent / Ph3P*Br2, Et3N / CH2Cl2 / 7 h 6: 1.) lithium amide / 1.) HMPTA, 15 deg C, 1.5 h, 2.) HMPTA, a) 0-10 deg C, 1 h, b) 20-25 deg C, 12 h 7: 91 percent / aq. HCl / acetone / 1 h / Heating 8: 95 percent / H2, NaBH4, Ni(CH3COO)2*4H2O, NH2(CH2)2NH2 / ethanol View Scheme
参考文献
Kovalev, V. G.; Nasser, Fadel Ahmed; Sorochinskaya, A. M.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 11.1 p. 1750 - 1753
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 11 p. 1664 - 1666
