1: With diisobutylaluminium hydride in dichloromethane; toluene
T=20°C; 24 h;
2: With sodium hydroxide in dichloromethane; toluene
T=20°C; 0.25 h; Further stages.;
参考文献
Zhang, Chen; De, Chandra Kanta; Mal, Rudrajit; Seidel, Daniel
Journal of the American Chemical Society, 2008 , vol. 130, # 2 p. 416 - 417
1: 180 °C
2: trichlorophosphate / 110 °C
View Scheme
参考文献
Bursavich, Matthew G.; Dastrup, David; Shenderovich, Mark; Yager, Kraig M.; Cimbora, Daniel M.; Williams, Brandi; Kumar, D. Vijay
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 24 p. 6829 - 6833