1,1,4,4-四乙氧基-2-丁炔合成路线 (共 14 条)
参考文献
Dunn, Peter J.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1579 - 1584
反应条件
formic acid T=25°C; 2.5 h;
参考文献
Gorgues, A.; Simon, A.; Coq, A. Le; Hercouet, A.; Corre, F.
Tetrahedron, 1986 , vol. 42, # 1 p. 351 - 370
反应条件
formic acid in chloroform T=40°C; 1 h; Yield given;
参考文献
Gorgues, A.; Simon, A.; Coq, A. Le; Hercouet, A.; Corre, F.
Tetrahedron, 1986 , vol. 42, # 1 p. 351 - 370
反应条件
formic acid T=25°C; 2.5 h;
参考文献
Gorgues, A.; Simon, A.; Coq, A. Le; Hercouet, A.; Corre, F.
Tetrahedron, 1986 , vol. 42, # 1 p. 351 - 370
反应条件
formic acid in chloroform T=15°C; 13 h;
参考文献
Saksena; Green; Mangiaracina; et al.
Tetrahedron Letters, 1985 , vol. 26, # 52 p. 6427 - 6430
反应条件
formic acid in chloroform T=40°C; 1 h; Yield given;
参考文献
Gorgues, A.; Simon, A.; Coq, A. Le; Hercouet, A.; Corre, F.
Tetrahedron, 1986 , vol. 42, # 1 p. 351 - 370
反应条件
zinc(II) chloride
T=170°C; P=11032.6 Torr;
参考文献
Howk; Sauer
Journal of the American Chemical Society, 1958 , vol. 80, p. 4607
Org. Synth. Coll. Vol., 1963 , vol. IV, p. 801
反应条件
1: propargyladehyde di-ethyl acetal With ethylmagnesium bromide in tetrahydrofuran; diethyl ether
T=-10°C; 2 h;
2: diethyl phenyl orthoformate in tetrahydrofuran; diethyl ether
T=-10 - 20°C;
参考文献
Albert, Sebastien; Soret, Adrien; Blanco, Luis; Deloisy, Sandrine
Tetrahedron, 2007 , vol. 63, # 13 p. 2888 - 2900
反应条件
manganese(IV) oxide; In(OSO2CF3)3 in chloroform
30 h; Heating;
参考文献
Smith, Brendan M.; Graham, Andrew E.
Tetrahedron Letters, 2007 , vol. 48, # 28 p. 4891 - 4894
反应条件
zinc(II) iodide
T=190°C; 2 h;
参考文献
Gorgues, A.; Simon, A.; Coq, A. Le; Hercouet, A.; Corre, F.
Tetrahedron, 1986 , vol. 42, # 1 p. 351 - 370