1,1,2,2-四乙氧基乙烷合成路线 (共 18 条)
反应条件
1: 65 percent / ZnCl2 / 3 h / 90 °C 2: K2CO3 / H2O View Scheme
参考文献
Stambouli, A.; Chastrette, F.; Amouroux, R.; Chastrette, M.; Mattioda, G.; Blanc, A.
Tetrahedron Letters, 1986 , vol. 27, # 35 p. 4149 - 4152
反应条件
1: 65 percent / ZnCl2 / 3 h / 90 °C 2: K2CO3 / H2O View Scheme
参考文献
Stambouli, A.; Chastrette, F.; Amouroux, R.; Chastrette, M.; Mattioda, G.; Blanc, A.
Tetrahedron Letters, 1986 , vol. 27, # 35 p. 4149 - 4152
反应条件
1: 65 percent / ZnCl2 / 3 h / 90 °C 2: NaOH / H2O / 1 h / Ambient temperature View Scheme
参考文献
Stambouli, A.; Chastrette, F.; Amouroux, R.; Chastrette, M.; Mattioda, G.; Blanc, A.
Tetrahedron Letters, 1986 , vol. 27, # 35 p. 4149 - 4152
反应条件
zinc(II) chloride T=90°C; 3 h;
参考文献
Stambouli, A.; Chastrette, F.; Amouroux, R.; Chastrette, M.; Mattioda, G.; Blanc, A.
Tetrahedron Letters, 1986 , vol. 27, # 35 p. 4149 - 4152
参考文献
Stambouli, A.; Amouroux, R.; Chastrette, F.; Chastrette, M.; Mattioda, G.; Blanc, A.
Journal of Organometallic Chemistry, 1986 , vol. 307, p. 139 - 144
反应条件
1: 65 percent / ZnCl2 / 3 h / 90 °C 2: 94 percent / LiAlH4 / diethyl ether / 2 h / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 35 p. 4149 - 4152
反应条件
zirconium sulphate; magnesium sulfate in chloroform; water
10 h; Heating;
参考文献
Sangsari, Farid Hamedi; Chastrette, Francine; Chastrette, Maurice
Synthetic Communications, 1988 , vol. 18, # 12 p. 1343 - 1348
反应条件
zirconium sulphate; magnesium sulfate in chloroform
2.5 h; Heatingfurther reagents, time; Product distribution;
参考文献
Sangsari, Farid Hamedi; Chastrette, Francine; Chastrette, Maurice
Synthetic Communications, 1988 , vol. 18, # 12 p. 1343 - 1348
参考文献
McElvain; Walters
Journal of the American Chemical Society, 1942 , vol. 64, p. 1964
Full Text Show Details
Pinner
Chemische Berichte, 1872 , vol. 5, p. 151
反应条件
2: durch Oxydation
3: NH4Cl; ethanol / im Rohr
View Scheme
参考文献
Fischer; Baer
Helvetica Chimica Acta, 1935 , vol. 18, p. 516