2,2,5,5-四甲基-4-苯基-3-咪唑-1-氧自由基合成路线 (共 8 条)
反应条件
hydrazine hydrate in ethanol T=20°C; 1 h;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 5 p. 1030 - 1035
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 5 p. 1140 - 1146
反应条件
manganese(IV) oxide; magnesium sulfate in tetrahydrofuran; diethyl ether 2 h;
参考文献
Grigor'ev; Bakunova; Kirilyuk
Russian Chemical Bulletin, 2000 , vol. 49, # 12 p. 2031 - 2036
反应条件
1: tetrahydrofuran; diethyl ether / 1 h / 20 °C 2: 95 mg / MnO2; MgSO4 / various solvent(s); diethyl ether; tetrahydrofuran / 2 h View Scheme
参考文献
Grigor'ev; Bakunova; Kirilyuk
Russian Chemical Bulletin, 2000 , vol. 49, # 12 p. 2031 - 2036
反应条件
1: tetrahydrofuran; diethyl ether / 1 h / 20 °C 2: 95 mg / MnO2; MgSO4 / various solvent(s); diethyl ether; tetrahydrofuran / 2 h View Scheme
参考文献
Grigor'ev; Bakunova; Kirilyuk
Russian Chemical Bulletin, 2000 , vol. 49, # 12 p. 2031 - 2036
反应条件
bromine in chloroform 1 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 7 p. 1275 - 1279
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1581 - 1586
反应条件
sodium hydroxide; C8H13Cl2N2O2 in ethanol
Yields of byproduct given;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 12 p. 2501 - 2509
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 12 p. 2787 - 2797
反应条件
sodium hydroxide in ethanol
Product distribution;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 12 p. 2501 - 2509
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 12 p. 2787 - 2797
反应条件
sodium hydroxide in ethanol
Product distribution;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 12 p. 2501 - 2509
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 12 p. 2787 - 2797