1-羟基-2,2,4,5,5-五甲基-3-咪唑啉合成路线 (共 9 条)
反应条件
1: LDA 2: MnO2 View Scheme
参考文献
Reznikov, V. A.; Reznikova, T. I.; Volodarskii, L. B.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1881 - 1888
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2135 - 2143
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Reznikov, V. A.; Reznikova, T. I.; Volodarskii, L. B.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1881 - 1888
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2135 - 2143
反应条件
triethylamine in methanol
20 h;
参考文献
Shchukin, G. I.; Grigor'ev, I. A.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 10 p. 2123 - 2127
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 10 p. 2357 - 2360
反应条件
1: 9 percent / N2H4*H2O / ethanol / 1 h / 20 °C
View Scheme
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 5 p. 1030 - 1035
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 5 p. 1140 - 1146
反应条件
ammonium hydroxide
T=20°C; 2 h;
参考文献
Sommer, Christian; Noeth, Heinrich; Ponikwar, Werner; Beck, Wolfgang
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2004 , vol. 59, # 6 p. 639 - 654
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 5 p. 1030 - 1035
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 5 p. 1140 - 1146
反应条件
in chloroform
T=19.9°C; ΔG; Equilibrium constantThermodynamic data;
参考文献
Dikanov, S. A.; Grigor'ev, I. A.; Volodarskii, L. B.; Tsvetkov, Yu. D.
Russian Journal of Physical Chemistry, 1982 , vol. 56, # 11 p. 1696 - 1699
Zhurnal Fizicheskoi Khimii, 1982 , vol. 56, # 11 p. 2762 - 2767
反应条件
in hexane
T=20°C; Rate constant;
参考文献
Malievskii, A. D.; Koroteev, S. V.; Volodarskii, L. B.; Shapiro, A. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 11 p. 2331 - 2338
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 11 p. 2575 - 2582
反应条件
1.) phenyllithium, ether, 1 h; 2.) lead dioxide, benzene, 12 h.; Yield given. Multistep reaction;
参考文献
Reznikov, V. A.; Reznikova, T. I.; Volodarskii, L. B.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1881 - 1888
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2135 - 2143