2-丙醇-1,1,1,3,3,3-d6合成路线 (共 9 条)
反应条件
lithium sulphate; [Ru(2,2':6':2''-terpyridine)(2,2'-bipyridine)O](2+) in water T=25.3°C; kinetic isotope effects; Mechanism;
参考文献
Casey, Charles P.; Johnson, Jeffrey B.
Journal of Organic Chemistry, 2003 , vol. 68, # 5 p. 1998 - 2001
反应条件
oxygen T=24.9°C; Irradiation; MechanismRate constant;
参考文献
Washida, Nobuaki
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3757 - 3764
反应条件
oxygen T=24.9°C; Irradiation; MechanismRate constant;
参考文献
Washida, Nobuaki
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3757 - 3764
反应条件
lithium aluminium tetrahydride in diethylene glycol dimethyl ether
T=0°C; Reduction; 1 h;
参考文献
Baldwin, Jack E.; Adlington, Robert M.; Crouch, Nicholas P.; Pereira, Ines A.C.
Journal of Labelled Compounds and Radiopharmaceuticals, 1998 , vol. 41, # 12 p. 1145 - 1163
反应条件
hydrogen; iron
T=22°C; P=2068.59 Torr; Title compound not separated from byproducts;
参考文献
Oezkart, Saim; Finke, Richard G.
Journal of the American Chemical Society, 2005 , vol. 127, # 13 p. 4800 - 4808
反应条件
trimethylamine-N-oxide; C18H26O4RuSi2 in water
Oppenauer-like oxidation; 18 h; Reflux;
参考文献
Moyer, Sara A.; Funk, Timothy W.
Tetrahedron Letters, 2010 , vol. 51, # 41 p. 5430 - 5433
反应条件
nickel
P=760 Torr; 1 h; Heating5h; Product distribution;
参考文献
Yamashita, Masaru; Dai, Feng-Yuen; Suzuki, Minoru; Saito, Yasukazu
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 2 p. 628 - 634
反应条件
hydrogen iodide in water
19 h; Heating;
参考文献
Sakamoto, Kenkichi; Tsutsui, Shinobu; Sakurai, Hideki; Kira, Mitsuo
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 1 p. 253 - 260
反应条件
hydrogen bromide
Heating;
参考文献
Braverman, Samuel; Duar, Ytzhak
Journal of the American Chemical Society, 1990 , vol. 112, # 15 p. 5830 - 5837