1-氨基-4-[(4-甲基苯基)氨基]蒽-9,10-二酮合成路线 (共 12 条)
反应条件
aluminium trichloride in nitrobenzene
Ambient temperature;
参考文献
Philip, George; Nabar, U. T.; Kanetkar, V. R.; Sunthankar, S. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 808 - 811
反应条件
in N,N-dimethyl-formamide
2 h; Heating;
参考文献
Gornostaev, L. M.; Zeibert, G. F.; Zolotareva, G. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 7 p. 704 - 707
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 7 p. 912 - 915
反应条件
1: 1) amyl nitrite 2) NaN3 / 1)acetic acid, room temperature 2) 30 min
2: toluene / 2 h / Heating
3: 95 percent / dimethylformamide / 2 h / Heating
View Scheme
参考文献
Gornostaev, L. M.; Zeibert, G. F.; Zolotareva, G. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 7 p. 704 - 707
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 7 p. 912 - 915
反应条件
boric acid
T=150 - 160°C;
参考文献
Bayer and Co.
Patent: DE125666 ;
参考文献
Gornostaev, L. M.; Es'kin, A. P.; Korniets, E. D.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2093 - 2096
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2344 - 2346
反应条件
1: toluene / 2 h / Heating
2: 95 percent / dimethylformamide / 2 h / Heating
View Scheme
参考文献
Gornostaev, L. M.; Zeibert, G. F.; Zolotareva, G. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 7 p. 704 - 707
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 7 p. 912 - 915
参考文献
Bayer and Co.
Patent: DE125578 ;
参考文献
Naiki et al.
Yuki Gosei Kagaku Kyokaishi, 1959 , vol. 17, p. 705,707
Chem.Abstr., 1960 , p. 1853
反应条件
Verseifen des Produkts durch Erwaermen mit Schwefelsaeure;
参考文献
Bayer and Co.
Patent: DE148767 ;
参考文献
Bayer and Co.
Patent: DE125666 ;