4-甲氧基-3,5-二甲基苯胺合成路线 （共 8 条）
参考文献
Research Development Foundation
Patent: US5674876 A1, 1997 ;
反应条件
1: HNO3; acetic acid anhydride 2: Raney nickel; diethyl ether / Hydrogenation View Scheme
参考文献
Baldwin; Robinson
Journal of the Chemical Society, 1934 , p. 1264,1266
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Rowe; Bannister; Storey
Journal of the Society of Chemical Industry, London, 1931 , vol. 50, p. 79 T
反应条件
1: ethanolic sodium ethylate 2: Raney nickel; diethyl ether / Hydrogenation View Scheme
参考文献
Bruice et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 83,87
反应条件
1: aqueous NaOH / Behandeln bei Siedetemperatur 2: glacial acetic acid; aqueous HNO3 / 60 - 70 °C 3: iron; aqueous hydrochloric acid View Scheme
参考文献
Baldwin; Robinson
Journal of the Chemical Society, 1934 , p. 1264,1266
反应条件
pyridine; aniline in dichloromethane
参考文献
Research Development Foundation
Patent: US5674876 A1, 1997 ;
反应条件
sulfuric acid; sodium nitrite Eintragen der Reaktionsloesung in siedende wss. HBr unter Zusatz von Cu2O;
参考文献
Bruice et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 83,87
反应条件
1: aqueous H2SO4; NaNO2 / Eintragen der Reaktionsloesung in siedende wss. HBr unter Zusatz von Cu2O 2: HNO3; H2SO4; acetic acid anhydride View Scheme
参考文献
Bruice et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 83,87
反应条件
sulfuric acid; sodium nitrite
Erwaermen der Reaktionsloesung mit wss. KI;
参考文献
Bielig; Luetzel
Justus Liebigs Annalen der Chemie, 1957 , vol. 608, p. 140,156
