1-(4-氟苯基)-4-硝基苯合成路线 （共 26 条）
反应条件
palladium diacetate in 1,4-dioxane
T=20°C; 2.5 h;
参考文献
Darses, Sylvain; Genet, Jean-Pierre; Brayer, Jean-Louis; Demoute, Jean-Pierre
Tetrahedron Letters, 1997 , vol. 38, # 25 p. 4393 - 4396
反应条件
caesium carbonate; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=60°C; Suzuki cross-coupling;
参考文献
Steiniger, Bjoern; Wuest, Frank R.
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 9 p. 817 - 827
反应条件
sodium hydroxide; tetrabutylammomium bromide; palladium on activated charcoal
T=100°C; Suzuki-Miyaura cross-coupling; 2 h;
参考文献
Lysen, Morten; Koehler, Klaus
Synthesis, 2006 , # 4 p. 692 - 698
反应条件
potassium fluoride in dimethyl sulfoxide
T=105°C; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Huang, Dan-Feng
European Journal of Organic Chemistry, 2010 , # 3 p. 416 - 419
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.166667 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
1: p-fluorophenylgermanium trichloride With ammonium hydroxide
T=20°C; 1 h;
2: para-nitro iodo-benzene With sodium hydroxide; palladium diacetate in 1,4-dioxane; water
4 h; Heating; Further stages.;
参考文献
Endo, Mayuko; Fugami, Keigo; Enokido, Tatsuki; Sano, Hiroshi; Kosugi, Masanori
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 7 p. 1025 - 1027
反应条件
palladium diacetate; triphenylphosphine; 2,2,2-trimethylacetic acid in 1-methyl-pyrrolidin-2-one
T=90°C; Suzuki Coupling; 4 h;
参考文献
Peng, Zhimin; Hu, Gaobo; Qiao, Hongwei; Xu, Pengxiang; Gao, Yuxing; Zhao, Yufen
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2733 - 2738
反应条件
1: N-(4-nitrophenyl)acetamide With boron trifluoride-methanol in methanol
T=65°C; Inert atmosphere;
2: With tert.-butylnitrite in methanol
T=0°C; 1 h; Inert atmosphere;
3: potassium (4-fluorophenyl)trifluoroborate With palladium diacetate in methanol
T=20°C; Suzuki Coupling; 12.25 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Berger, Rene
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 463 - 476
反应条件
tris-(dibenzylideneacetone)dipalladium(0); copper(I) bromide dimethylsulfide complex; trifuran-2-yl-phosphane in tetrahydrofuran
Stille coupling; Heating;
参考文献
Dubbaka, Srinivas Reddy; Vogel, Pierre
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15292 - 15293
反应条件
potassium fluoride; dibenzo-18-crown-6; tetraphthaloyl chloride in sulfolane
T=200°C; 23 h;
参考文献
Effenberger, Franz; Streicher, Willi
Chemische Berichte, 1991 , vol. 124, # 1 p. 157 - 162
