您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-三氟甲基联苯
合成路线
（共 170 条）
13041-70-8
4-溴-反-二苯乙烯
+
402-43-7
对溴三氟甲苯
+
23665-09-0
苯基碘化锌
→
反应条件
21175-18-8
+
398-36-7
4-三氟甲基联苯
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in tetrahydrofuran; toluene T=40°C; 0.5 h; Reagent/catalyst; Overall yield = 58 percent;
参考文献
Shirakawa, Eiji; Tamakuni, Fumiko; Kusano, Eugene; Uchiyama, Nanase; Konagaya, Wataru; Watabe, Ryo; Hayashi, Tamio
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 521 - 525
Angew. Chem., 2014 , vol. 126, # 2 p. 531 - 535,5
462-06-6
氟苯
+
95752-87-7
+
501374-30-7
→
反应条件
1137-79-7
N,N-二甲基-4-联苯胺
+
398-36-7
4-三氟甲基联苯
反应条件
[Ni0(1,5-cyclooctadiene)2]; zirconium (IV) fluoride; cesium fluoride; tri-cyclo-hexyl-phosphine in toluene T=20 - 100°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Xu, Tian; Shimasaki, Toshiaki; Chatani, Naoto
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19505 - 19511
108-86-1
溴代苯
+
95752-87-7
+
501374-30-7
→
反应条件
1137-79-7
N,N-二甲基-4-联苯胺
+
398-36-7
4-三氟甲基联苯
反应条件
[Ni0(1,5-cyclooctadiene)2]; cesium fluoride; tri-cyclo-hexyl-phosphine in toluene T=20 - 100°C; Suzuki-Miyaura coupling; 2 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Xu, Tian; Shimasaki, Toshiaki; Chatani, Naoto
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19505 - 19511
591-50-4
碘苯
+
95752-87-7
+
501374-30-7
→
反应条件
1137-79-7
N,N-二甲基-4-联苯胺
+
398-36-7
4-三氟甲基联苯
反应条件
[Ni0(1,5-cyclooctadiene)2]; cesium fluoride; tri-cyclo-hexyl-phosphine in toluene T=20 - 100°C; Suzuki-Miyaura coupling; 2 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Xu, Tian; Shimasaki, Toshiaki; Chatani, Naoto
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19505 - 19511
108-90-7
+
95752-87-7
+
501374-30-7
→
反应条件
1137-79-7
N,N-二甲基-4-联苯胺
+
398-36-7
4-三氟甲基联苯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [Ni0(1,5-cyclooctadiene)2]; cesium fluoride in toluene T=20 - 100°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Tobisu, Mamoru; Xu, Tian; Shimasaki, Toshiaki; Chatani, Naoto
Journal of the American Chemical Society, 2011 , vol. 133, # 48 p. 19505 - 19511
54527-55-8
→
反应条件
398-36-7
4-三氟甲基联苯
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / -30 - 0 °C 1.2: 0 - 20 °C 2.1: F5I*C5H5N*FH / dichloromethane / 24 h / 20 °C View Scheme
参考文献
Hara, Shoji; Monoi, Miki; Umemura, Ryosuke; Fuse, Chiaki
Tetrahedron, 2012 , vol. 68, # 49 p. 10145 - 10150,6
108-86-1
溴代苯
+
21856-96-2
→
反应条件
119-61-9
+
92-52-4
+
728-86-9
+
398-36-7
4-三氟甲基联苯
反应条件
palladium diacetate; caesium carbonate; tri-cyclo-hexyl-phosphine in o-xylene 22 h; Heating; Title compound not separated from byproducts;
参考文献
Terao, Yoshito; Wakui, Hiroyuki; Nomoto, Michiyo; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5236 - 5243
69231-87-4
→
反应条件
398-36-7
4-三氟甲基联苯
反应条件
pyridine; palladium diacetate; potassium carbonate T=120°C; 6 h; Ionic liquid;
参考文献
Xin, Bingwei; Jia, Chunxiao; Qi, Zhixun
Journal of Chemical Research, 2012 , vol. 36, # 7 p. 407 - 410
92-67-1
→
反应条件
398-36-7
4-三氟甲基联苯
反应条件
1.1: tert.-butylnitrite / water; ethanol / 1 h / 0 - 20 °C / |Inert atmosphere 2.1: copper(I) isothiocyanate; caesium carbonate / acetonitrile / 0.17 h / 20 °C / |Inert atmosphere 2.2: 16 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Danoun, Gregory; Bayarmagnai, Bilguun; Gruenberg, Matthias F.; Goossen, Lukas J.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 31 p. 7972 - 7975
Angew. Chem., 2013 , vol. 125, # 31 p. 8130 - 8133
4049-96-1
+
455-13-0
→
反应条件
581-80-6
+
398-36-7
4-三氟甲基联苯
反应条件
1: diallyl(diphenyl)germane With antimony(V) fluoride on graphite in toluene Inert atmosphereHeating; 2: 4-trifluoromethyl-1-iodobenzene With tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; toluene 18 h; Inert atmosphereHeating; chemoselective reaction;
参考文献
Pitteloud, Jean-Philippe; Liang, Yong; Wnuk, Stanislaw F.
Chemistry Letters, 2011 , vol. 40, # 9 p. 967 - 969
首页
上一页
1
...
13
14
15
16
17
下一页
末页
到第
页
确定
