1: With sodium dithionite; triethylamine in ethanol; water
T=50°C; 1.5 h;
2: With hydrogenchloride in ethanol; water
T=60°C; 1 h; Product distribution / selectivity;
参考文献
TEMPLE UNIVERSITY - OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION; MOUNT SINAI SCHOOL OF MEDICINE; REDDY, E., Premkumar; REDDY, M. V., Ramana
Patent: WO2012/166586 A1, 2012 ;
Location in patent: Page/Page column 74 ;
WO 2012/166586 A1
1.1: sodium hydroxide / ethanol / 0.08 h / 20 °C
1.2: 1 h / Reflux
2.1: triethylamine; sodium dithionite / ethanol; water / 1.5 h / 50 °C
2.2: 1 h / 60 °C
View Scheme
参考文献
TEMPLE UNIVERSITY - OF THE COMMONWEALTH SYSTEM OF HIGHER EDUCATION; MOUNT SINAI SCHOOL OF MEDICINE; REDDY, E., Premkumar; REDDY, M. V., Ramana
Patent: WO2012/166586 A1, 2012 ;
WO 2012/166586 A1
