2-苯基噁唑-4-羧酸乙酯合成路线 （共 36 条）
反应条件
1: LiAlH4 / diethyl ether 2: SOCl2 View Scheme
参考文献
Jansen,A.B.A.; Szelke,M.
Journal of the Chemical Society, 1961 , p. 405 - 411
反应条件
1: LiAlH4 / diethyl ether 2: PBr5 / benzene 3: methanol / Heating View Scheme
参考文献
Jansen,A.B.A.; Szelke,M.
Journal of the Chemical Society, 1961 , p. 405 - 411
反应条件
1: With lithium hydroxide; water in tetrahydrofuran T=23°C; 2: With hydrogenchloride in water pH=2 - 3;
参考文献
VICURON PHARMACEUTICALS INC.
Patent: US2006/211603 A1, 2006 ;
Location in patent: Page/Page column 71 ;
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in toluene
T=90°C; Suzuki-Miyaura reaction; 1 h;
参考文献
Hodgetts, Kevin J.; Kershaw, Mark T.
Organic Letters, 2002 , vol. 4, # 17 p. 2905 - 2907
反应条件
palladium diacetate; caesium carbonate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane
T=110°C; 18 h; Inert atmosphere; Reagent/catalyst;
参考文献
Theveau, Laure; Querolle, Olivier; Dupas, Georges; Hoarau, Christophe
Tetrahedron, 2013 , vol. 69, # 22 p. 4375 - 4380
反应条件
palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane
T=110°C; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Theveau, Laure; Verrier, Cecile; Lassalas, Pierrik; Martin, Thibaut; Dupas, Georges; Querolle, Olivier; Van Hijfte, Luc; Marsais, Francis; Hoarau, Christophe
Chemistry - A European Journal, 2011 , vol. 17, # 51 p. 14450 - 14463
反应条件
P(t-Bu)2Me*HBF4; palladium diacetate; caesium carbonate in 1,4-dioxane
T=110°C; 18 h; Inert atmosphere; Reagent/catalyst;
参考文献
Theveau, Laure; Querolle, Olivier; Dupas, Georges; Hoarau, Christophe
Tetrahedron, 2013 , vol. 69, # 22 p. 4375 - 4380
反应条件
palladium diacetate; caesium carbonate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane
T=110°C; 18 h; Inert atmosphere; Reagent/catalyst;
参考文献
Theveau, Laure; Querolle, Olivier; Dupas, Georges; Hoarau, Christophe
Tetrahedron, 2013 , vol. 69, # 22 p. 4375 - 4380
反应条件
silver hexafluoroantimonate in 1,2-dichloro-ethane
T=90°C; 2 h; Inert atmosphereMicrowave irradiation;
参考文献
Ritson, Dougal J.; Spiteri, Christian; Moses, John E.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3519 - 3522
反应条件
palladium diacetate; potassium carbonate; biphenyl-2-yl-di-tert-butyl-phosphane; 2,2,2-trimethylacetic acid in 1,4-dioxane
T=110°C; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Theveau, Laure; Verrier, Cecile; Lassalas, Pierrik; Martin, Thibaut; Dupas, Georges; Querolle, Olivier; Van Hijfte, Luc; Marsais, Francis; Hoarau, Christophe
Chemistry - A European Journal, 2011 , vol. 17, # 51 p. 14450 - 14463
