2-苯基噁唑-4-羧酸乙酯合成路线 (共 36 条)
反应条件
T=170°C; 0.0166667 h;
参考文献
Yokoyama, Masataka; Irie, Masakazu; Sujino, Keiko; Kagemoto, Tsukusi; Togo, Hideo; Funabashi, Masuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 16 p. 2127 - 2134
反应条件
1: sodium hydride; 18-crown-6 ether / toluene / 20 - 60 °C / |Cooling with ice
2: triethylamine; triphenylphosphine; iodine / dichloromethane / 3 h / 20 °C
View Scheme
参考文献
Khose, Goraksha; Shinde, Shailesh; Panmand, Anil; Kulkarni, Ravibhushan; Munot, Yogesh; Bandyopadhyay, Anish; Barawkar, Dinesh; Patil, Santoshkumar N.
Tetrahedron Letters, 2014 , vol. 55, # 16 p. 2671 - 2674
反应条件
1: 100 percent / triethylamine / 0.17 h / Ambient temperature
2: 22 percent / 0.02 h / 170 °C / other alkyl O-vinylcarbohydroximates, sugar lactoxime O-vinyl ethers
View Scheme
参考文献
Yokoyama, Masataka; Irie, Masakazu; Sujino, Keiko; Kagemoto, Tsukusi; Togo, Hideo; Funabashi, Masuo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 16 p. 2127 - 2134
反应条件
1: 86 percent / N-bromosuccinimide / CHCl3 / 48 h / Heating
2: 91 percent / K2CO3 / Pd(PPh3)4 / H2O; toluene / 90 °C
3: 95 percent / NaOH / ethanol / 20 °C
4: 74 percent / dimethylformamide; H2O / 60 h / 150 °C
View Scheme
参考文献
Hodgetts, Kevin J.; Kershaw, Mark T.
Organic Letters, 2002 , vol. 4, # 17 p. 2905 - 2907
反应条件
1: LiAlH4 / diethyl ether
2: PBr5 / benzene
View Scheme
参考文献
Jansen,A.B.A.; Szelke,M.
Journal of the Chemical Society, 1961 , p. 405 - 411
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Jansen,A.B.A.; Szelke,M.
Journal of the Chemical Society, 1961 , p. 405 - 411