2-羟基-5-硝基苯甲腈合成路线 （共 26 条）
反应条件
in dimethyl sulfoxide
T=100 - 120°C;
参考文献
Gorvin, John H.
Journal of Chemical Research, Miniprint, 1991 , # 4 p. 738 - 762
参考文献
Auwers; Walker
Chemische Berichte, 1898 , vol. 31, p. 3041
反应条件
potassium fluoride in acetonitrile
1.) r.t., 2.) reflux, overnight;
参考文献
Clark, James H.; Tavener, Stewart J.
Journal of Fluorine Chemistry, 1997 , vol. 85, # 2 p. 169 - 172
反应条件
potassium fluoride; tetra-phenylphosphonium bromide in acetonitrile
1.) r.t., 2.) reflux, overnight;
参考文献
Clark, James H.; Tavener, Stewart J.
Journal of Fluorine Chemistry, 1997 , vol. 85, # 2 p. 169 - 172
参考文献
Lindemann; Thiele
Justus Liebigs Annalen der Chemie, 1926 , vol. 449, p. 75
反应条件
sodium hydroxide
0.166667 h; Heating; Yield given;
参考文献
Corsaro, Antonino; Buemi, Giuseppe; Chiacchio, Ugo; Perrini, Giancarlo; Pistara, Venerando; Romeo, Roberto
Tetrahedron, 1996 , vol. 52, # 23 p. 7885 - 7892
反应条件
formic acid; hydroxylamine hydrochloride
Heating;
参考文献
Lambert, Stephanie G.; Taylor, Jo-Anne M.; Wegener, Kate L.; Woodhouse, Susan L.; Lincoln, Stephen F.; Ward, A. David
New Journal of Chemistry, 2000 , vol. 24, # 7 p. 541 - 546
反应条件
2: 5percent aq. NaOH / 0.17 h / Heating
View Scheme
参考文献
Corsaro, Antonino; Buemi, Giuseppe; Chiacchio, Ugo; Perrini, Giancarlo; Pistara, Venerando; Romeo, Roberto
Tetrahedron, 1996 , vol. 52, # 23 p. 7885 - 7892
反应条件
1: natrium carbonate; alcohol; hydroxylamine hydrochloride
2: concentrated hydrochloric acid
3: NaOH-solution
View Scheme
参考文献
Brady; Bishop
Journal of the Chemical Society, 1925 , vol. 127, p. 1362
反应条件
potassium fluoride
Ambient temperatureother temp.; Product distribution;
参考文献
Clark, James H.; Tavener, Stewart J.
Journal of Fluorine Chemistry, 1997 , vol. 85, # 2 p. 169 - 172
