(9ci)-1-甲基-1H-咪唑-2-乙腈合成路线 （共 7 条）
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the Chemical Society, , p. 3305
反应条件
in dimethyl sulfoxide
Heating;
参考文献
Liao, Chen; Zhu, Xiang; Sun, Xiao-Guang; Dai, Sheng
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5308 - 5310
反应条件
in N,N-dimethyl-formamide
T=45°C; 4 h;
参考文献
Alcalde, Ermitas; Alemany, Montserrat; Gisbert, Maria
Tetrahedron, 1996 , vol. 52, # 48 p. 15171 - 15188
反应条件
in dichloromethane; water; dimethyl sulfoxide
参考文献
Merck and Co., Inc.
Patent: US4746669 A1, 1988 ;
反应条件
1: 86 percent / thionyl chloride / CH2Cl2 / 5 h / Ambient temperature
2: 87 percent / dimethylformamide / 4 h / 45 °C
View Scheme
参考文献
Alcalde, Ermitas; Alemany, Montserrat; Gisbert, Maria
Tetrahedron, 1996 , vol. 52, # 48 p. 15171 - 15188
反应条件
1: 66 percent / NaBH4 / methanol / 20 h / Ambient temperature
2: 86 percent / thionyl chloride / CH2Cl2 / 5 h / Ambient temperature
3: 87 percent / dimethylformamide / 4 h / 45 °C
View Scheme
参考文献
Alcalde, Ermitas; Alemany, Montserrat; Gisbert, Maria
Tetrahedron, 1996 , vol. 52, # 48 p. 15171 - 15188
反应条件
sodium azide; ammonium chloride in N,N-dimethyl-formamide
T=120 - 130°C; 17 h;
参考文献
Reese, Colin B.; Pei-Zhuo, Zhang
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 19 p. 2291 - 2302
