2-二甲基氨基乙基硬脂酸酯合成路线 （共 7 条）
反应条件
in ethanol T=100°C; 3 h;
参考文献
Kao Corporation
Patent: US2005/90423 A1, 2005 ;
Location in patent: Page/Page column 6-7 ;
反应条件
in ethanol T=100°C; 3 h;
参考文献
Kao Corporation
Patent: US2005/90423 A1, 2005 ;
Location in patent: Page/Page column 6-7 ;
反应条件
in acetonitrile 0.25 h; Heating;
参考文献
Detert; Seifert; Schunack
Pharmazie, 1996 , vol. 51, # 2 p. 67 - 72
反应条件
in diethyl ether
1) cooling, 30 min, 2) r.t., 1 h;
参考文献
Detert; Seifert; Schunack
Pharmazie, 1996 , vol. 51, # 2 p. 67 - 72
反应条件
T=150 - 180°C; 14 h;
参考文献
Kao Corporation
Patent: US2005/90423 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
4-(N,N-dimethlyamino)pyridine; dicyclohexyl-carbodiimide in dichloromethane; benzene
T=0 - 20°C; Inert atmosphere;
参考文献
Tarafdar, Pradip K.; Reddy, S. Thirupathi; Swamy, Musti J.
Journal of Physical Chemistry B, 2013 , vol. 117, # 34 p. 9900 - 9909
反应条件
1: oxalyl dichloride / dichloromethane / 0.08 h / 65 °C
2: acetonitrile / 0.08 h / 20 °C
View Scheme
参考文献
Li, Xingnan; Franke, Adrian A.
Analytical Chemistry, 2011 , vol. 83, # 8 p. 3192 - 3198
