N-[(7S)-4-(羟基甲基)-1,2,3,10-四甲氧基-9-氧代-6,7-二氢-5H-苯并[d]庚搭烯-7-基]乙酰胺合成路线 （共 3 条）
反应条件
sodium tetrahydroborate in methanol
T=20°C; 3 h; Inert atmosphere;
参考文献
Nishiyama, Hiroyuki; Ono, Masahiro; Sugimoto, Takuya; Sasai, Toshio; Asakawa, Naoyuki; Ueno, Satoshi; Tominaga, Yoshitaka; Yaegashi, Takashi; Nagaoka, Masato; Matsuzaki, Takeshi; Kogure, Noriyuki; Kitajima, Mariko; Takayama, Hiromitsu
MedChemComm, 2014 , vol. 5, # 4 p. 452 - 458
反应条件
sulfuric acid; water
T=20°C; 0.666667 h;
参考文献
Bensel, Nicolas; Lagnoux, David; Niggli, Verena; Wartmann, Markus; Reymond, Jean-Louis
Helvetica Chimica Acta, 2004 , vol. 87, # 9 p. 2266 - 2272
反应条件
1: tin(IV) chloride / dichloromethane / 20 °C
2: sodium tetrahydroborate / methanol / 3 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Nishiyama, Hiroyuki; Ono, Masahiro; Sugimoto, Takuya; Sasai, Toshio; Asakawa, Naoyuki; Ueno, Satoshi; Tominaga, Yoshitaka; Yaegashi, Takashi; Nagaoka, Masato; Matsuzaki, Takeshi; Kogure, Noriyuki; Kitajima, Mariko; Takayama, Hiromitsu
MedChemComm, 2014 , vol. 5, # 4 p. 452 - 458
