4-(2-氯丙-2-基)-1-甲基环己烯合成路线 (共 32 条)
反应条件
2,4,6-trimethyl-pyridine 8 h; Heating; Title compound not separated from byproducts;
参考文献
Ishihara; Nakamura; Yamamoto
Synlett, 2001 , # 7 p. 1113 - 1116
反应条件
1: zinc(II) isothiocyanate With titanium tetrachloride in dichloromethane 0.166667 h; ultrasound irradiation; 2: α-terpinyl chloride With pyridine in dichloromethane T=25°C; 6 h; ultrasound irradiation;
参考文献
Bettadaiah; Gurudutt; Srinivas
Synthetic Communications, 2003 , vol. 33, # 13 p. 2293 - 2299
反应条件
pyridine; zinc(II) chloride other alkyl halides, other time, and solv.; Product distribution;
参考文献
Gurudutt; Rao; Srinivas
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 3 p. 343 - 344
反应条件
1: zinc(II) isothiocyanate With titanium tetrachloride in dichloromethane 0.166667 h; ultrasound irradiation; 2: α-terpinyl chloride With pyridine in dichloromethane T=25°C; 6 h; ultrasound irradiation;
参考文献
Synthetic Communications, , vol. 33, # 13 p. 2293 - 2299
反应条件
pyridine; zinc(II) chloride other alkyl halides, other time, and solv.; Product distribution;
参考文献
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 3 p. 343 - 344
反应条件
d-limonene monohydrochloride;
参考文献
Wallach; Kremers
Justus Liebigs Annalen der Chemie, 1892 , vol. 270, p. 189
反应条件
titanium tetrachloride; N-methylaniline in dichloromethane
T=-23°C; 1 h;
参考文献
Itoh, Akira; Saito, Tadashi; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 5 p. 1456 - 1459
反应条件
hydrogenchloride; carbon disulfide
参考文献
Hercules Powder Co.
Patent: US2394359 , 1941 ;
反应条件
1: With potassium hydride in 1,4-dioxane
Inert atmosphere;
2: With niobium pentachloride in 1,4-dioxane
Inert atmosphere;
参考文献
Ravikumar; Yao, Lihua; Fleming, Fraser F.
Journal of Organic Chemistry, 2009 , vol. 74, # 19 p. 7294 - 7299
反应条件
1: With potassium hydride in 1,4-dioxane
Inert atmosphere;
2: With niobium pentachloride in 1,4-dioxane
Inert atmosphere;
参考文献
Ravikumar; Yao, Lihua; Fleming, Fraser F.
Journal of Organic Chemistry, 2009 , vol. 74, # 19 p. 7294 - 7299