2-(2-噻吩基硫)噻吩合成路线 (共 55 条)
反应条件
diethyl ether; sulfur
参考文献
Challenger; Harrison
J. Inst. Petr. Technol., 1935 , vol. 21, p. 135,153
反应条件
sulenium monochloride
1.) tetrahydrofuran, reflux, 2 h, 2.) tetrahydrofuran, 3 h; Yield given. Multistep reaction;
参考文献
Bertini, Vincenzo; Munno, Angela De; Picci, Nevio; Lucchesini, Francesco; Pocci, Marco
Heterocycles, 1987 , vol. 26, # 8 p. 2153 - 2158
反应条件
dimethyl selenide; hydrogen sulfide in gas
T=500°C; effect of dimethyl selenide on reaction; various temperatures; Product distributionMechanism;
参考文献
Korchevin, N. A.; Papernaya, L. K.; Ostroukhova, L. A.; Sukhomazova, E. N.; Efremova, G. G.; at al.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 9 p. 2087 - 2091,1841 - 1844
反应条件
in gas
thermolysis above 380 deg C;
参考文献
Korchevin, N. A.; Sukhomazova, E. N.; Russavskaya, N. V.; Turchaninova, L. P.; Sigalov, M. V.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1991 , vol. 27, # 10 p. 1049 - 1052
Khimiya Geterotsiklicheskikh Soedinenii, 1991 , vol. 27, # 10 p. 1312 - 1316
反应条件
Kinetics; byproducts: HCl; at 500-600°C;
参考文献
Voronkov, M. G.; Deryagina, E. N.
Phosphorus Sulfur, 1979 , vol. 7, p. 123 - 132
Full Text Show Details
Gmelin Handbook: S: SVol.4a/b, 1.3.11.7, page 302 - 302
Full Text Show Details
Voronkov, M. G.; Deryagina, E. N.
Top. Org. Sulphur Chem. Plenary Lect. 8th Intern. Symp., Portoroz, Yugosl., 1978, pp. 363/87
反应条件
hydrogen sulfide
T=130°C; 7 h; other temperatures, reaction time; Product distribution;
参考文献
Voronkov, M. G.; Deryagina, E. N.; Papernaya, L. K.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 2580 - 2582
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 12 p. 2783 - 2785
反应条件
methanol; hydrogen sulfide
T=610°C; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Deryagina; Sukhomazova; Levanova
Chemistry of Heterocyclic Compounds, 2002 , vol. 38, # 1 p. 40 - 45
反应条件
T=550°C; 0.0141667 h; gas phase copyrolysis; Product distribution;
参考文献
Voronkov, M. G.; Deryagina, E. N.; Sukhomazova, E. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1516 - 1522
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1736 - 1743
反应条件
oxygen
Product distribution;
参考文献
Vvedenskii, V. Yu.; Zinchenko, S. V.; Shkarupa, T. A.; Korchevin, N. A.; Deryagina, E. N.; Voronkov, M. G.
Doklady Chemistry, 1989 , vol. 305, # 1-6 p. 98 - 100
Dokl. Akad. Nauk SSSR Ser. Khim., 1989 , vol. 305, # 3 p. 624 - 627
反应条件
T=500 - 550°C; Product distribution;
参考文献
Voronkov, M. G.; Deryagina, E. N.; Papernaya, L. K.; Sukhomazova, E. N.; Korchevin, N. A.; Efremova, G. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 12 p. 1301 - 1306
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 12 p. 1614 - 1619