(4-甲氧基苯乙炔基)三甲基硅烷合成路线 （共 73 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=20°C; 1 h;
参考文献
Zhou, Ningzhang; Wang, Li; Thompson, David W.; Zhao, Yuming
Tetrahedron, 2011 , vol. 67, # 1 p. 125 - 143
反应条件
copper(l) iodide; diisopropylamine; bis(benzonitrile)palladium(II) dichloride in 1,4-dioxane T=20°C; Sonogashira coupling;
参考文献
Hill, Lensey L.; Smith, Joanna M.; Brown, William S.; Moore, Lucas R.; Guevera, Paul; Pair, Emily S.; Porter, Jake; Chou, Joe; Wolterman, Christopher J.; Craciun, Raluca; Dixon, David A.; Shaughnessy, Kevin H.
Tetrahedron, 2008 , vol. 64, # 29 p. 6920 - 6934
反应条件
zinc(II) chloride in 1,4-dioxane T=100°C; 1.5 h;
参考文献
Andreev, Aleksey A.; Konshin, Valeri V.; Komarov, Nikolai V.; Rubin, Michael; Brouwer, Chad; Gevorgyan, Vladimir
Organic Letters, 2004 , vol. 6, # 3 p. 421 - 424
反应条件
tin(II) trifluoromethanesulfonate; triethylamine in dichloromethane 3 h; Ambient temperature;
参考文献
Yamaguchi, Masahiko; Hayashi, Akio; Minami, Toru
Journal of Organic Chemistry, 1991 , vol. 56, # 13 p. 4091 - 4092
反应条件
triethylamine; acetone in 2,2,2-trifluoroethanol 60 h; Irradiation;
参考文献
Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 35 p. 5675 - 5678
反应条件
zinc trifluoromethanesulfonate; triethylamine in dichloromethane T=23°C; 0.75 h;
参考文献
Rahaim Jr., Ronald J.; Shaw, Jared T.
Journal of Organic Chemistry, 2008 , vol. 73, # 7 p. 2912 - 2915
反应条件
triethylamine in 2,2,2-trifluoroethanol 36 h; Irradiation;
参考文献
Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 35 p. 5675 - 5678
反应条件
triethylamine in 2,2,2-trifluoroethanol 60 h; Irradiation;
参考文献
Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Angewandte Chemie - International Edition, 2005 , vol. 44, # 35 p. 5675 - 5678
反应条件
1: ZTK-2-125 With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=-78°C; 1 h;
参考文献
Araki, Yuta; Kobayashi, Koji; Yonemoto, Misato; Kondo, Yoshinori
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 1 p. 78 - 80
反应条件
tetrabutylammomium bromide; palladium dichloride in water T=100°C; 8 h; Title compound not separated from byproducts;
参考文献
Alonso, Diego A.; Najera, Carmen; Pacheco, Ma. Carmen
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 9-10 p. 1146 - 1158
