(2S)-2-[[(2R)-2-氨基-3-甲基丁酰基]氨基]-4-甲基戊酸合成路线 (共 5 条)
反应条件
hydrogen; palladium in water; acetic acid; tert-butyl alcohol
Yield given;
参考文献
Oya, Masanao; Takahashi, Tomoko
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 9 p. 2705 - 2707
反应条件
1: triethylamine / acetonitrile / 4 h / 20 °C
2: H2 / Pd / acetic acid; 2-methyl-propan-2-ol; H2O
View Scheme
参考文献
Oya, Masanao; Takahashi, Tomoko
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 9 p. 2705 - 2707
反应条件
1: triethylamine / acetonitrile / 4 h / 20 °C
2: H2 / Pd / acetic acid; 2-methyl-propan-2-ol; H2O
View Scheme
参考文献
Oya, Masanao; Takahashi, Tomoko
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 9 p. 2705 - 2707
反应条件
hydrogenchloride; hydrogen; palladium in methanol
参考文献
Luebke,K.; Schroeder,E.
Justus Liebigs Annalen der Chemie, 1963 , vol. 665, p. 205 - 212
反应条件
1: (i) ClCO2Et, Et3N, THF, (ii) /BRN= 3586583/, DMF
2: H2, aq. HCl / Pd / methanol
View Scheme
参考文献
Luebke,K.; Schroeder,E.
Justus Liebigs Annalen der Chemie, 1963 , vol. 665, p. 205 - 212