2,3-二氢-1H-吲哚-3-羧酸甲酯合成路线 （共 4 条）
反应条件
trifluoroacetic acid in dichloromethane
T=20°C; Inert atmosphere;
参考文献
Pietruszka, Joerg; Simon, Robert Christian
Chemistry - A European Journal, 2010 , vol. 16, # 48 p. 14534 - 14544
反应条件
1.1: sodium hydride / tetrahydrofuran / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: magnesium / methanol; dichloromethane / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
View Scheme
参考文献
Pietruszka, Joerg; Simon, Robert Christian
Chemistry - A European Journal, 2010 , vol. 16, # 48 p. 14534 - 14544
反应条件
1: magnesium / methanol; dichloromethane / Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 20 °C / Inert atmosphere
View Scheme
参考文献
Pietruszka, Joerg; Simon, Robert Christian
Chemistry - A European Journal, 2010 , vol. 16, # 48 p. 14534 - 14544
反应条件
thionyl chloride
T=67°C; Cooling with ice;
参考文献
Alatorre-Santamaria, Sergio; Gotor-Fernandez, Vicente; Gotor, Vicente
Tetrahedron Asymmetry, 2010 , vol. 21, # 18 p. 2307 - 2313
